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000837456 1001_ $$0P:(DE-Juel1)144465$$aBuchholz, Martin$$b0
000837456 245__ $$aOptimized separation procedure for production of no-carrier-added radiomanganese for positron emission tomography
000837456 260__ $$aBerlin$$bDe Gruyter$$c2015
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000837456 520__ $$aThe natCr(p, xn)-process is a very efficient route for production of 52gMn (T1/2 = 5.59 d). Based on measurements of distribution coefficients with different media and ion-exchange resins, an optimized chromatographic separation of radiomanganese from natCr with the resin Amberlite CG400 was developed. With this system natCr is eluted first with an acetic acid/methanol 1:1 mixture at room temperature and 52gMn thereafter with 3 M HCl at 50 ℃. Within a separation time of 4 h the method yielded 99.5% of the n.c.a. 52gMn in 2–3 mL of 3 M HCl. An ICP-MS analysis revealed a chromium impurity of 0.07 mg (0.014%) in the n.c.a. 52gMn solution, making this separation method suitable for the production of 52gMn for medical applications like positron emission tomography (PET).
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000837456 7001_ $$0P:(DE-Juel1)131849$$aSpahn, Ingo$$b1$$eCorresponding author
000837456 7001_ $$0P:(DE-Juel1)131816$$aCoenen, Heinrich Hubert$$b2$$ufzj
000837456 773__ $$0PERI:(DE-600)2039575-9$$a10.1515/ract-2015-2506$$gVol. 103, no. 12$$n12$$p7$$tRadiochimica acta$$v103$$x2193-3405$$y2015
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