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@ARTICLE{Buchholz:837456,
      author       = {Buchholz, Martin and Spahn, Ingo and Coenen, Heinrich
                      Hubert},
      title        = {{O}ptimized separation procedure for production of
                      no-carrier-added radiomanganese for positron emission
                      tomography},
      journal      = {Radiochimica acta},
      volume       = {103},
      number       = {12},
      issn         = {2193-3405},
      address      = {Berlin},
      publisher    = {De Gruyter},
      reportid     = {FZJ-2017-06369},
      pages        = {7},
      year         = {2015},
      abstract     = {The natCr(p, xn)-process is a very efficient route for
                      production of 52gMn (T1/2 = 5.59 d). Based on
                      measurements of distribution coefficients with different
                      media and ion-exchange resins, an optimized chromatographic
                      separation of radiomanganese from natCr with the resin
                      Amberlite CG400 was developed. With this system natCr is
                      eluted first with an acetic acid/methanol 1:1 mixture at
                      room temperature and 52gMn thereafter with 3 M HCl at
                      50 ℃. Within a separation time of 4 h the method
                      yielded $99.5\%$ of the n.c.a. 52gMn in 2–3 mL of 3 M
                      HCl. An ICP-MS analysis revealed a chromium impurity of
                      0.07 mg $(0.014\%)$ in the n.c.a. 52gMn solution, making
                      this separation method suitable for the production of 52gMn
                      for medical applications like positron emission tomography
                      (PET).},
      cin          = {INM-5},
      ddc          = {540},
      cid          = {I:(DE-Juel1)INM-5-20090406},
      pnm          = {573 - Neuroimaging (POF3-573)},
      pid          = {G:(DE-HGF)POF3-573},
      typ          = {PUB:(DE-HGF)16},
      UT           = {WOS:000366187300008},
      doi          = {10.1515/ract-2015-2506},
      url          = {https://juser.fz-juelich.de/record/837456},
}