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| Home > Publications database > Optimized separation procedure for production of no-carrier-added radiomanganese for positron emission tomography > print |
| 001 | 837456 | ||
| 005 | 20210129231336.0 | ||
| 024 | 7 | _ | |a 10.1515/ract-2015-2506 |2 doi |
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| 037 | _ | _ | |a FZJ-2017-06369 |
| 041 | _ | _ | |a English |
| 082 | _ | _ | |a 540 |
| 100 | 1 | _ | |a Buchholz, Martin |0 P:(DE-Juel1)144465 |b 0 |
| 245 | _ | _ | |a Optimized separation procedure for production of no-carrier-added radiomanganese for positron emission tomography |
| 260 | _ | _ | |a Berlin |c 2015 |b De Gruyter |
| 336 | 7 | _ | |a article |2 DRIVER |
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| 336 | 7 | _ | |a Journal Article |0 0 |2 EndNote |
| 520 | _ | _ | |a The natCr(p, xn)-process is a very efficient route for production of 52gMn (T1/2 = 5.59 d). Based on measurements of distribution coefficients with different media and ion-exchange resins, an optimized chromatographic separation of radiomanganese from natCr with the resin Amberlite CG400 was developed. With this system natCr is eluted first with an acetic acid/methanol 1:1 mixture at room temperature and 52gMn thereafter with 3 M HCl at 50 ℃. Within a separation time of 4 h the method yielded 99.5% of the n.c.a. 52gMn in 2–3 mL of 3 M HCl. An ICP-MS analysis revealed a chromium impurity of 0.07 mg (0.014%) in the n.c.a. 52gMn solution, making this separation method suitable for the production of 52gMn for medical applications like positron emission tomography (PET). |
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| 700 | 1 | _ | |a Spahn, Ingo |0 P:(DE-Juel1)131849 |b 1 |e Corresponding author |
| 700 | 1 | _ | |a Coenen, Heinrich Hubert |0 P:(DE-Juel1)131816 |b 2 |u fzj |
| 773 | _ | _ | |a 10.1515/ract-2015-2506 |g Vol. 103, no. 12 |0 PERI:(DE-600)2039575-9 |n 12 |p 7 |t Radiochimica acta |v 103 |y 2015 |x 2193-3405 |
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