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000837512 1001_ $$0P:(DE-HGF)0$$aSkripnikova, Tatiana A.$$b0$$eCorresponding author
000837512 245__ $$aTowards stabilization of the potential response of Mn(III) tetraphenylporphyrin-based solid-state electrodes with selectivity for salicylate ions
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000837512 520__ $$aWe report a new type of solid-state electrode (type I) of a simple design with polyvinyl chloride membranes based on Mn(III) tetraphenylporphyrin and with graphite as the electronically conducting substrate. Enlargement of the membrane/graphite contact area by soaking graphite in the plasticizer with subsequent conditioning of the electrode at 30 °C allowed us to shorten the time required to achieve steady potential values of the sensors to just 3 days. These electrodes do not require a specially added RedOx system in the transducer layer. Stabilization of the EMF response of type I electrodes is compared to type II electrodes which contain a Cu0/Cu2+ RedOx couple in the transducer layer. Type I sensors are suitable for measuring the salicylate ion concentration in the clinically important concentration range down to 2.5 × 10−4 M with a sensitivity to salicylate ion of −59.0 mV decade−1 in solutions with a high constant background of chloride ions of 0.12 M at pH = 5.3, making this a promising technique for an effective design of solid-contact ion-selective electrodes with polymeric sensing membranes.
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000837512 7001_ $$0P:(DE-HGF)0$$aStarikova, Anna A.$$b1
000837512 7001_ $$0P:(DE-HGF)0$$aShumilova, Galina I.$$b2
000837512 7001_ $$0P:(DE-HGF)0$$aErmolenko, Yuri E.$$b3
000837512 7001_ $$0P:(DE-HGF)0$$aPendin, Andrey A.$$b4
000837512 7001_ $$0P:(DE-Juel1)128710$$aMourzina, Youlia$$b5$$eCorresponding author
000837512 773__ $$0PERI:(DE-600)1478940-1$$a10.1007/s10008-017-3575-6$$gVol. 21, no. 8, p. 2269 - 2279$$n8$$p2269 - 2279$$tJournal of solid state electrochemistry$$v21$$x1433-0768$$y2017
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