Hauptseite > Publikationsdatenbank > Towards stabilization of the potential response of Mn(III) tetraphenylporphyrin-based solid-state electrodes with selectivity for salicylate ions > print

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024 7 _ |a 10.1007/s10008-017-3575-6
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024 7 _ |a 1433-0768
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082 _ _ |a 540
100 1 _ |a Skripnikova, Tatiana A.
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245 _ _ |a Towards stabilization of the potential response of Mn(III) tetraphenylporphyrin-based solid-state electrodes with selectivity for salicylate ions
260 _ _ |a Berlin
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|b Springer
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520 _ _ |a We report a new type of solid-state electrode (type I) of a simple design with polyvinyl chloride membranes based on Mn(III) tetraphenylporphyrin and with graphite as the electronically conducting substrate. Enlargement of the membrane/graphite contact area by soaking graphite in the plasticizer with subsequent conditioning of the electrode at 30 °C allowed us to shorten the time required to achieve steady potential values of the sensors to just 3 days. These electrodes do not require a specially added RedOx system in the transducer layer. Stabilization of the EMF response of type I electrodes is compared to type II electrodes which contain a Cu0/Cu2+ RedOx couple in the transducer layer. Type I sensors are suitable for measuring the salicylate ion concentration in the clinically important concentration range down to 2.5 × 10−4 M with a sensitivity to salicylate ion of −59.0 mV decade−1 in solutions with a high constant background of chloride ions of 0.12 M at pH = 5.3, making this a promising technique for an effective design of solid-contact ion-selective electrodes with polymeric sensing membranes.
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700 1 _ |a Starikova, Anna A.
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700 1 _ |a Shumilova, Galina I.
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700 1 _ |a Ermolenko, Yuri E.
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700 1 _ |a Pendin, Andrey A.
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700 1 _ |a Mourzina, Youlia
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773 _ _ |a 10.1007/s10008-017-3575-6
|g Vol. 21, no. 8, p. 2269 - 2279
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|t Journal of solid state electrochemistry
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