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@ARTICLE{Krause:837518,
author = {Krause, Kay J. and Brings, Fabian and Schnitker, Jan and
Kätelhön, Enno and Rinklin, Philipp and Mayer, Dirk and
Compton, Richard G. and Lemay, Serge G. and Offenhäusser,
Andreas and Wolfrum, Bernhard},
title = {{T}he {I}nfluence of {S}upporting {I}ons on the
{E}lectrochemical {D}etection of {I}ndividual {S}ilver
{N}anoparticles: {U}nderstanding the {S}hape and {F}requency
of {C}urrent {T}ransients in {N}ano-impacts},
journal = {Chemistry - a European journal},
volume = {23},
number = {19},
issn = {0947-6539},
address = {Weinheim},
publisher = {Wiley-VCH},
reportid = {FZJ-2017-06414},
pages = {4638 - 4643},
year = {2017},
abstract = {We report the influence of electrolyte composition and
concentration on the stochastic amperometric detection of
individual silver nanoparticles at microelectrode arrays and
show that the sensor response at certain electrode
potentials is dependent on both the conductivity of the
electrolyte and the concentration of chloride ions. We
further demonstrate that the chloride concentration in
solution heavily influences the characteristic current spike
shape of recorded nanoparticle impacts: While typically too
short to be resolved in the measured current, the spike
widths are significantly broadened at low chloride
concentrations below 10 mm and range into the millisecond
regime. The analysis of more than 25 000 spikes reveals
that this effect can be explained by the diffusive mass
transport of chloride ions to the nanoparticle, which limits
the oxidation rate of individual silver nanoparticles to
silver chloride at the chosen electrode potential.},
cin = {ICS-8 / PGI-8},
ddc = {540},
cid = {I:(DE-Juel1)ICS-8-20110106 / I:(DE-Juel1)PGI-8-20110106},
pnm = {523 - Controlling Configuration-Based Phenomena (POF3-523)},
pid = {G:(DE-HGF)POF3-523},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000399326500016},
pubmed = {pmid:28182315},
doi = {10.1002/chem.201605924},
url = {https://juser.fz-juelich.de/record/837518},
}