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@ARTICLE{Winkler:837855,
author = {Winkler, Florian and Tavabi, Amir Hossein and Barthel, Juri
and Duchamp, Martial and Yucelen, Emrah and Borghardt, Sven
and Kardynal, Beata and Dunin-Borkowski, Rafal},
title = {{Q}uantitative measurement of mean inner potential and
specimen thickness from high-{R}esolution off-axis electron
holograms of ultrathin layered {WS}e2},
journal = {Ultramicroscopy},
volume = {178},
issn = {0304-3991},
address = {Amsterdam},
publisher = {Elsevier Science},
reportid = {FZJ-2017-06632},
pages = {38 - 47},
year = {2017},
abstract = {The phase and amplitude of the electron wavefunction that
has passed through ultra-thin flakes of WSe2 is measured
from high-resolution off-axis electron holograms. Both the
experimental measurements and corresponding computer
simulations are used to show that, as a result of dynamical
diffraction, the spatially averaged phase does not increase
linearly with specimen thickness close to an [001] zone axis
orientation even when the specimen has a thickness of only a
few layers. It is then not possible to infer the local
specimen thickness of the WSe2 from either the phase or the
amplitude alone. Instead, we show that the combined analysis
of phase and amplitude from experimental measurements and
simulations allows an accurate determination of the local
specimen thickness. The relationship between phase and
projected potential is shown to be approximately linear for
extremely thin specimens that are tilted by several degrees
in certain directions from the [001] zone axis. A knowledge
of the specimen thickness then allows the electrostatic
potential to be determined from the measured phase. By using
this combined approach, we determine a value for the mean
inner potential of WSe2 of 18.9±0.8 V, which is $12\%$
lower than the value calculated from neutral atom scattering
factors.},
cin = {ER-C-1 / PGI-5},
ddc = {570},
cid = {I:(DE-Juel1)ER-C-1-20170209 / I:(DE-Juel1)PGI-5-20110106},
pnm = {143 - Controlling Configuration-Based Phenomena (POF3-143)},
pid = {G:(DE-HGF)POF3-143},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000403862900007},
doi = {10.1016/j.ultramic.2016.07.016},
url = {https://juser.fz-juelich.de/record/837855},
}