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@ARTICLE{Gunkel:837945,
author = {Gunkel, Felix and Jin, Lei and Müller, David and Hausner,
Clemens and Bick, Daniel S. and Jia, Chun-Lin and Schneller,
Theodor and Valov, Ilia and Waser, R. and Dittmann, Regina},
title = {{O}rdering and {P}hase {C}ontrol in {E}pitaxial
{D}ouble-{P}erovskite {C}atalysts for the {O}xygen
{E}volution {R}eaction},
journal = {ACS catalysis},
volume = {7},
issn = {2155-5435},
address = {Washington, DC},
publisher = {ACS},
reportid = {FZJ-2017-06706},
pages = {7029 - 7037},
year = {2017},
abstract = {The complex oxide compound praseodymium barium cobalt oxide
(PBCO) is an efficient catalyst for the oxygen evolution
reaction (OER) during electrochemical water splitting, with
an activity that is mainly ascribed to PBCO’s inherent
atomic structure and band alignment. Here, we report on
epitaxial PBCO thin films showing electrocatalytic
properties, with current densities of up to 10 mA/cm2 at 1.8
V vs RHE. Dense PBCO thin films are synthesized in a
disordered perovskite phase as well as in a coherently
oxygen vacancy ordered (double) perovskite phase, in which
oxygen vacancies are incorporated in every second CoO2−δ
atomic plane along the out-of-plane direction. The
transition from disordered to ordered growth occurs with
temperature control during the growth process and can be
directly monitored in situ by means of reflection
high-energy electron diffraction. The epitaxial fabrication
process allows the control of the structure and phase of the
oxide catalysts, providing model systems for exploring
structure–property relations and atomistic processes of
catalysis during the OER. For all structural compositions,
we demonstrate remarkably similar catalytic properties,
indicating a negligible effect of the structural bulk phase
on OER catalysis. Rational design routes for perovskite
catalysts derived merely from bulk properties should
therefore be met with suspicion.},
cin = {PGI-7 / JARA-FIT / IEK-9 / ER-C-1 / PGI-6},
ddc = {540},
cid = {I:(DE-Juel1)PGI-7-20110106 / $I:(DE-82)080009_20140620$ /
I:(DE-Juel1)IEK-9-20110218 / I:(DE-Juel1)ER-C-1-20170209 /
I:(DE-Juel1)PGI-6-20110106},
pnm = {524 - Controlling Collective States (POF3-524)},
pid = {G:(DE-HGF)POF3-524},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000412795700071},
doi = {10.1021/acscatal.7b02036},
url = {https://juser.fz-juelich.de/record/837945},
}