% IMPORTANT: The following is UTF-8 encoded. This means that in the presence
% of non-ASCII characters, it will not work with BibTeX 0.99 or older.
% Instead, you should use an up-to-date BibTeX implementation like “bibtex8” or
% “biber”.
@PHDTHESIS{Weidlich:838348,
author = {Weidlich, Sabrina},
title = {{N}anoscale 3{D} structures towards improved cell-chip
coupling on microelectrode arrays},
volume = {156},
school = {RWTH Aachen University},
type = {Dr.},
address = {Jülich},
publisher = {Forschungszentrum Jülich GmbH Zentralbibliothek, Verlag},
reportid = {FZJ-2017-06973},
isbn = {978-3-95806-278-8},
series = {Schriften des Forschungszentrums Jülich. Reihe
Schlüsseltechnologien / Key Technologies},
pages = {II, 154 S.},
year = {2017},
note = {RWTH Aachen, Diss., 2017},
abstract = {The human brain is a highly interconnected system,
consisting of about 86 billion neurons,$^{[1]}$ each forming
on average 7,000 connections to neighboring cells.$^{[2]}$
While neuroscientists have achieved various breakthroughs
elucidating the underlying principles of neuronal
communication in the past decades, the goal of an in-depth
understanding of the complex events involved in network
communication and processes such as learning remains
unattained. One approach often employed to reduce the
complexity and thereby facilitate high-resolution studies of
the cellular interactionis the application of microelectrode
arrays (MEAs). They enable the $\textit{in vitro}$
investigation of small neuronal networks, yielding
correlated data of the cellular activity with high temporal
resolution. However, MEAs suffer from inherently low signal
amplitudes due to a loose cell-chip contact and thus
insufficient coupling between the cellular signals and the
electrode. In the past decade, three dimensional electrode
designs have been extensively studied as possible solution
for the problem of low signal amplitudes during MEA-based
investigations of electrogenic cells. They improve the
cell-chip coupling through the establishment of a tighter
interface between biology and electronics. However, while
many different 3D designs have been suggested in the
literature, the requirements for a direct comparison of the
recording capabilities yielded by the different structures
have so far not been met. The aim of this body of work
therefore is the development of an approach allowing for the
parallel fabrication of multiple different 3D designs on a
single chip and thus parallel testing on the biological
system. In the first part of this thesis, electron-beam
lithography is employed in conjunction with electrode
position for a parallelized preparation of thousands of 3D
structures on gold-on-silicon substrates. In this manner,
the common 3D geometries as reported in the literature -
pillars, hollow pillars, and mushroom-shaped structures -
are produced. Furthermore, hollow mushrooms are developed as
novel 3D design. The interaction of the structures with both
cardiomyocyte-like HL-1 cells as well as rat cortical
neurons is investigated. In the second part of this thesis,
the developed 3D structures are transferred onto MEAs. A
thorough investigation of the galvanization procedure yields
parameters that enable the real-time control of the
nanoscale structure size during the electrode position
process. In this way, 3D electrodes of different shape and
size can be prepared on a single MEA and thus be
investigated simultaneously with respect to their
interaction with electrogenic cells. Electrophysiological
studies are performed employing cardiomyocyte-like HL-1
cells as model system. Furthermore, various modifications of
the 3D structures are discussed, aiming at improved
electrical characteristics for future investigations. In
conclusion, this body of work presents a well-controlled
process for the preparation of 3D structures on MEAs,
thereby facilitating the preparation of multiple different
three-dimensional designs on a single chip. This forms the
basis for an in-depth characterization of the improvement of
the cell-chip coupling yielded by the different 3D designs.},
cin = {ICS-8},
cid = {I:(DE-Juel1)ICS-8-20110106},
pnm = {552 - Engineering Cell Function (POF3-552)},
pid = {G:(DE-HGF)POF3-552},
typ = {PUB:(DE-HGF)3 / PUB:(DE-HGF)11},
urn = {urn:nbn:de:0001-2017121335},
url = {https://juser.fz-juelich.de/record/838348},
}