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@ARTICLE{Blass:839949,
      author       = {Blass, Johanna and Brunke, Jessica and Emmerich, Franziska
                      and Przybylski, Cédric and Garamus, Vasil M and Feoktystov,
                      Artem and Bennewitz, Roland and Wenz, Gerhard and Albrecht,
                      Marcel},
      title        = {{I}nteractions between shape-persistent macromolecules as
                      probed by {AFM}},
      journal      = {Beilstein journal of organic chemistry},
      volume       = {13},
      issn         = {1860-5397},
      address      = {Frankfurt, Main},
      publisher    = {Beilstein-Institut zur Förderung der Chemischen
                      Wissenschaften},
      reportid     = {FZJ-2017-07526},
      pages        = {938 - 951},
      year         = {2017},
      abstract     = {Water-soluble shape-persistent cyclodextrin (CD) polymers
                      with amino-functionalized end groups were prepared starting
                      from diacetylene-modified cyclodextrin monomers by a
                      combined Glaser coupling/click chemistry approach.
                      Structural perfection of the neutral CD polymers and
                      inclusion complex formation with ditopic and monotopic guest
                      molecules were proven by MALDI–TOF and UV–vis
                      measurements. Small-angle neutron and X-ray (SANS/SAXS)
                      scattering experiments confirm the stiffness of the polymer
                      chains with an apparent contour length of about 130 Å.
                      Surface modification of planar silicon wafers as well as AFM
                      tips was realized by covalent bound formation between the
                      terminal amino groups of the CD polymer and a reactive
                      isothiocyanate–silane monolayer. Atomic force measurements
                      of CD polymer decorated surfaces show enhanced
                      supramolecular interaction energies which can be attributed
                      to multiple inclusion complexes based on the rigidity of the
                      polymer backbone and the regular configuration of the CD
                      moieties. Depending on the geometrical configuration of
                      attachment anisotropic adhesion characteristics of the
                      polymer system can be distinguished between a peeling and a
                      shearing mechanism.},
      cin          = {JCNS (München) ; Jülich Centre for Neutron Science JCNS
                      (München) ; JCNS-FRM-II / JCNS-2 / PGI-4},
      ddc          = {540},
      cid          = {I:(DE-Juel1)JCNS-FRM-II-20110218 /
                      I:(DE-Juel1)JCNS-2-20110106 / I:(DE-Juel1)PGI-4-20110106},
      pnm          = {6G15 - FRM II / MLZ (POF3-6G15) / 6G4 - Jülich Centre for
                      Neutron Research (JCNS) (POF3-623)},
      pid          = {G:(DE-HGF)POF3-6G15 / G:(DE-HGF)POF3-6G4},
      experiment   = {EXP:(DE-MLZ)KWS1-20140101},
      typ          = {PUB:(DE-HGF)16},
      pubmed       = {pmid:28684975},
      UT           = {WOS:000405164300001},
      doi          = {10.3762/bjoc.13.95},
      url          = {https://juser.fz-juelich.de/record/839949},
}