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000840163 1001_ $$0P:(DE-HGF)0$$aMarcos Esteban, Raquel$$b0
000840163 245__ $$aSynthesis of ruthenium@graphene nanomaterials in propylene carbonate as re-usable catalysts for the solvent-free hydrogenation of benzene
000840163 260__ $$aAmsterdam [u.a.]$$bElsevier$$c2015
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000840163 500__ $$aDedicated to Prof. Ekkehard Hahn on the occasion of his 60th birthday
000840163 520__ $$aRuthenium nanoparticles (Ru-NPs) can be deposited on thermally reduced graphite oxide (TRGO) in propylene carbonate (PC). Propylene carbonate is a biodegradable and non-toxic solvent. Synthesis of Ru-NPs and deposition on TRGO were achieved by decomposition of ruthenium dodecacarbonyl, Ru3(CO)12, by microwave irradiation. Ru@graphene nanomaterials were identified and characterized by high resolution transmission electron microscopy (TEM, HR-TEM), energy-dispersive X-ray diffraction (EDX), selected area electron diffraction (SAED), X-ray photoelectron spectroscopy (XPS) and powder X-ray diffraction (PXRD) with a small diameter and size distribution of Ru-NPs on TRGO. These Ru@graphene nanomaterials are active catalysts for the solvent-free hydrogenation of benzene to cyclohexane under mild conditions (100 °C, 10 bar) with activities of and over 90% conversion in at least ten consecutive runs.
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000840163 7001_ $$0P:(DE-HGF)0$$aSchütte, Kai$$b1
000840163 7001_ $$0P:(DE-HGF)0$$aMarquardt, Dorothea$$b2
000840163 7001_ $$0P:(DE-Juel1)130525$$aBarthel, Juri$$b3
000840163 7001_ $$0P:(DE-HGF)0$$aBeckert, Fabian$$b4
000840163 7001_ $$0P:(DE-HGF)0$$aMülhaupt, Rolf$$b5
000840163 7001_ $$00000-0002-6288-9605$$aJaniak, Christoph$$b6$$eCorresponding author
000840163 773__ $$0PERI:(DE-600)2825222-6$$a10.1016/j.nanoso.2015.07.002$$gVol. 2, p. 28 - 34$$p28 - 34$$tNano-structures & nano-objects$$v2$$x2352-507X$$y2015
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