Home > Publications database > Synthesis of ruthenium@graphene nanomaterials in propylene carbonate as re-usable catalysts for the solvent-free hydrogenation of benzene > print

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024 7 _ |a 10.1016/j.nanoso.2015.07.002
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037 _ _ |a FZJ-2017-07718
082 _ _ |a 530
100 1 _ |a Marcos Esteban, Raquel
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245 _ _ |a Synthesis of ruthenium@graphene nanomaterials in propylene carbonate as re-usable catalysts for the solvent-free hydrogenation of benzene
260 _ _ |a Amsterdam [u.a.]
|c 2015
|b Elsevier
336 7 _ |a article
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500 _ _ |a Dedicated to Prof. Ekkehard Hahn on the occasion of his 60th birthday
520 _ _ |a Ruthenium nanoparticles (Ru-NPs) can be deposited on thermally reduced graphite oxide (TRGO) in propylene carbonate (PC). Propylene carbonate is a biodegradable and non-toxic solvent. Synthesis of Ru-NPs and deposition on TRGO were achieved by decomposition of ruthenium dodecacarbonyl, Ru3(CO)12, by microwave irradiation. Ru@graphene nanomaterials were identified and characterized by high resolution transmission electron microscopy (TEM, HR-TEM), energy-dispersive X-ray diffraction (EDX), selected area electron diffraction (SAED), X-ray photoelectron spectroscopy (XPS) and powder X-ray diffraction (PXRD) with a small diameter and size distribution of Ru-NPs on TRGO. These Ru@graphene nanomaterials are active catalysts for the solvent-free hydrogenation of benzene to cyclohexane under mild conditions (100 °C, 10 bar) with activities of and over 90% conversion in at least ten consecutive runs.
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700 1 _ |a Schütte, Kai
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700 1 _ |a Marquardt, Dorothea
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700 1 _ |a Barthel, Juri
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700 1 _ |a Beckert, Fabian
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700 1 _ |a Mülhaupt, Rolf
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700 1 _ |a Janiak, Christoph
|0 0000-0002-6288-9605
|b 6
|e Corresponding author
773 _ _ |a 10.1016/j.nanoso.2015.07.002
|g Vol. 2, p. 28 - 34
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|p 28 - 34
|t Nano-structures & nano-objects
|v 2
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