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000840169 1001_ $$0P:(DE-HGF)0$$aWegner, Susann$$b0
000840169 245__ $$aSoft wet-chemical synthesis of Ru-Sn nanoparticles from single-source ruthenocene-stannole precursors in an ionic liquid
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000840169 520__ $$aMicrowave-induced decomposition of the single-source precursors of a neutral triple-decker ruthenocene (1) and an anionic ruthenocene (2) both bearing a stannole ligand in the ionic liquid 1-butyl-3-methylimidazolium tetrafluoroborate ([BMIm][BF4]) gives bimetallic ruthenium-tin nanoparticles. Particles of approximate composition Ru2Sn (from 1) and Ru3Sn7 (from 2) were obtained in this soft, wet-chemical synthesis. Transmission electron microscopy (TEM) showed the formation of 2–6 nm particles of Ru2Sn with its average elemental composition determined from energy dispersive X-ray spectroscopy (EDX). Crystalline Ru3Sn7 nanoparticles together with α-Sn nanoparticles of 10–50 nm (from TEM) were elucidated by positive matching of the powder-X-ray diffractogram to the Ru3Sn7 and α-Sn phase and the element composition from EDX.
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000840169 7001_ $$0P:(DE-HGF)0$$aSaito, Masaichi$$b1
000840169 7001_ $$0P:(DE-Juel1)130525$$aBarthel, Juri$$b2
000840169 7001_ $$00000-0002-6288-9605$$aJaniak, Christoph$$b3$$eCorresponding author
000840169 773__ $$0PERI:(DE-600)1491530-3$$a10.1016/j.jorganchem.2016.05.010$$gVol. 821, p. 192 - 196$$p192 - 196$$tJournal of organometallic chemistry$$v821$$x0022-328X$$y2016
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