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@ARTICLE{Wegner:840169,
      author       = {Wegner, Susann and Saito, Masaichi and Barthel, Juri and
                      Janiak, Christoph},
      title        = {{S}oft wet-chemical synthesis of {R}u-{S}n nanoparticles
                      from single-source ruthenocene-stannole precursors in an
                      ionic liquid},
      journal      = {Journal of organometallic chemistry},
      volume       = {821},
      issn         = {0022-328X},
      address      = {New York, NY [u.a.]},
      publisher    = {Elsevier},
      reportid     = {FZJ-2017-07724},
      pages        = {192 - 196},
      year         = {2016},
      abstract     = {Microwave-induced decomposition of the single-source
                      precursors of a neutral triple-decker ruthenocene (1) and an
                      anionic ruthenocene (2) both bearing a stannole ligand in
                      the ionic liquid 1-butyl-3-methylimidazolium
                      tetrafluoroborate ([BMIm][BF4]) gives bimetallic
                      ruthenium-tin nanoparticles. Particles of approximate
                      composition Ru2Sn (from 1) and Ru3Sn7 (from 2) were obtained
                      in this soft, wet-chemical synthesis. Transmission electron
                      microscopy (TEM) showed the formation of 2–6 nm particles
                      of Ru2Sn with its average elemental composition determined
                      from energy dispersive X-ray spectroscopy (EDX). Crystalline
                      Ru3Sn7 nanoparticles together with α-Sn nanoparticles of
                      10–50 nm (from TEM) were elucidated by positive matching
                      of the powder-X-ray diffractogram to the Ru3Sn7 and α-Sn
                      phase and the element composition from EDX.},
      cin          = {ER-C-2},
      ddc          = {540},
      cid          = {I:(DE-Juel1)ER-C-2-20170209},
      pnm          = {143 - Controlling Configuration-Based Phenomena (POF3-143)},
      pid          = {G:(DE-HGF)POF3-143},
      typ          = {PUB:(DE-HGF)16},
      UT           = {WOS:000387633400024},
      doi          = {10.1016/j.jorganchem.2016.05.010},
      url          = {https://juser.fz-juelich.de/record/840169},
}