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000840189 1001_ $$00000-0002-1075-4194$$aSchmitz, Alexa$$b0
000840189 245__ $$aSynthesis of metal-fluoride nanoparticles supported on thermally reduced graphite oxide
000840189 260__ $$aFrankfurt, M.$$bBeilstein-Institut zur Förderung der Chemischen Wissenschaften$$c2017
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000840189 520__ $$aMetal-fluoride nanoparticles, (MFx-NPs) with M = Fe, Co, Pr, Eu, supported on different types of thermally reduced graphite oxide (TRGO) were obtained by microwave-assisted thermal decomposition of transition-metal amidinates, (M{MeC[N(iPr)]2}n) or [M(AMD)n] with M = Fe(II), Co(II), Pr(III), and tris(2,2,6,6-tetramethyl-3,5-heptanedionato)europium, Eu(dpm)3, in the presence of TRGO in the ionic liquid (IL) 1-butyl-3-methylimidazolium tetrafluoroborate ([BMIm][BF4]). The crystalline phases of the metal fluorides synthesized in [BMIm][BF4] were identified by powder X-ray diffraction (PXRD) to be MF2 for M = Fe, Co and MF3 for M = Eu, Pr. The diameters and size distributions of MFx@TRGO were from (6 ± 2) to (102 ± 41) nm. Energy-dispersive X-ray spectroscopy (EDX) and X-ray photoelectron spectroscopy (XPS) were used for further characterization of the MFx-NPs. Electrochemical investigations of the FeF2-NPs@TRGO as cathode material for lithium-ion batteries were evaluated by galvanostatic charge/discharge profiles. The results indicate that the FeF2-NPs@TRGO as cathode material can present a specific capacity of 500 mAh/g at a current density of 50 mA/g, including a significant interfacial charge storage contribution. The obtained nanomaterials show a good rate capacity as well (220 mAh/g and 130 mAh/g) at a current density of 200 and 500 mA/g, respectively.
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000840189 7001_ $$0P:(DE-HGF)0$$aSchütte, Kai$$b1
000840189 7001_ $$0P:(DE-HGF)0$$aIlievski, Vesko$$b2
000840189 7001_ $$0P:(DE-Juel1)130525$$aBarthel, Juri$$b3
000840189 7001_ $$0P:(DE-HGF)0$$aBurk, Laura$$b4
000840189 7001_ $$0P:(DE-HGF)0$$aMülhaupt, Rolf$$b5
000840189 7001_ $$0P:(DE-HGF)0$$aYue, Junpei$$b6
000840189 7001_ $$00000-0001-8452-2663$$aSmarsly, Bernd$$b7
000840189 7001_ $$00000-0002-6288-9605$$aJaniak, Christoph$$b8$$eCorresponding author
000840189 773__ $$0PERI:(DE-600)2583584-1$$a10.3762/bjnano.8.247$$gVol. 8, p. 2474 - 2483$$p2474 - 2483$$tBeilstein journal of nanotechnology$$v8$$x2190-4286$$y2017
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