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@ARTICLE{Schmitz:840189,
      author       = {Schmitz, Alexa and Schütte, Kai and Ilievski, Vesko and
                      Barthel, Juri and Burk, Laura and Mülhaupt, Rolf and Yue,
                      Junpei and Smarsly, Bernd and Janiak, Christoph},
      title        = {{S}ynthesis of metal-fluoride nanoparticles supported on
                      thermally reduced graphite oxide},
      journal      = {Beilstein journal of nanotechnology},
      volume       = {8},
      issn         = {2190-4286},
      address      = {Frankfurt, M.},
      publisher    = {Beilstein-Institut zur Förderung der Chemischen
                      Wissenschaften},
      reportid     = {FZJ-2017-07744},
      pages        = {2474 - 2483},
      year         = {2017},
      abstract     = {Metal-fluoride nanoparticles, (MFx-NPs) with M = Fe, Co,
                      Pr, Eu, supported on different types of thermally reduced
                      graphite oxide (TRGO) were obtained by microwave-assisted
                      thermal decomposition of transition-metal amidinates,
                      (M{MeC[N(iPr)]2}n) or [M(AMD)n] with M = Fe(II), Co(II),
                      Pr(III), and
                      tris(2,2,6,6-tetramethyl-3,5-heptanedionato)europium,
                      Eu(dpm)3, in the presence of TRGO in the ionic liquid (IL)
                      1-butyl-3-methylimidazolium tetrafluoroborate ([BMIm][BF4]).
                      The crystalline phases of the metal fluorides synthesized in
                      [BMIm][BF4] were identified by powder X-ray diffraction
                      (PXRD) to be MF2 for M = Fe, Co and MF3 for M = Eu, Pr. The
                      diameters and size distributions of MFx@TRGO were from (6 ±
                      2) to (102 ± 41) nm. Energy-dispersive X-ray spectroscopy
                      (EDX) and X-ray photoelectron spectroscopy (XPS) were used
                      for further characterization of the MFx-NPs. Electrochemical
                      investigations of the FeF2-NPs@TRGO as cathode material for
                      lithium-ion batteries were evaluated by galvanostatic
                      charge/discharge profiles. The results indicate that the
                      FeF2-NPs@TRGO as cathode material can present a specific
                      capacity of 500 mAh/g at a current density of 50 mA/g,
                      including a significant interfacial charge storage
                      contribution. The obtained nanomaterials show a good rate
                      capacity as well (220 mAh/g and 130 mAh/g) at a current
                      density of 200 and 500 mA/g, respectively.},
      cin          = {ER-C-2},
      ddc          = {620},
      cid          = {I:(DE-Juel1)ER-C-2-20170209},
      pnm          = {143 - Controlling Configuration-Based Phenomena (POF3-143)},
      pid          = {G:(DE-HGF)POF3-143},
      typ          = {PUB:(DE-HGF)16},
      UT           = {WOS:000416166400002},
      doi          = {10.3762/bjnano.8.247},
      url          = {https://juser.fz-juelich.de/record/840189},
}