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@ARTICLE{Raijmakers:841133,
author = {Raijmakers, L. H. J. and Lammers, M. J. G. and Notten, P.
H. L.},
title = {{A} new method to compensate impedance artefacts for
{L}i-ion batterieswith integrated micro-reference
electrodes},
journal = {Electrochimica acta},
volume = {259},
issn = {0013-4686},
address = {New York, NY [u.a.]},
publisher = {Elsevier},
reportid = {FZJ-2017-08233},
pages = {517 - 533},
year = {2018},
abstract = {In order to measure the electrochemical characteristics of
both electrodes inside Li-ion batteries, micro-reference
electrodes (μREF) turned out to be very useful. However,
measuring the electrochemical impedance with respect to
μREF can lead to severe measurement artefacts, making a
detailed analysis of the impedance spectra complicated. In
the present work a new method is developed in which
high-frequency measurement artefacts can be compensated. A
theoretical analysis, using equivalent circuit models of the
measurement setups, shows that if two different impedance
measurements are averaged, the impedance contributions from
the measurement leads can be completely eliminated. The
theoretical analysis is validated using Li-ion batteries
with seven integrated μREF, having all different
impedances. The measurement results show that artefacts are
dominating for high-impedance μREF in the high frequency
range. However, these artefacts can be fully compensated by
averaging two separate impedance measurements, as predicted
by theory. This easily makes it possible to perform
artefact-free impedance measurements, even at high
frequencies.},
cin = {IEK-9},
ddc = {540},
cid = {I:(DE-Juel1)IEK-9-20110218},
pnm = {131 - Electrochemical Storage (POF3-131)},
pid = {G:(DE-HGF)POF3-131},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000423968600058},
doi = {10.1016/j.electacta.2017.10.132},
url = {https://juser.fz-juelich.de/record/841133},
}