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@ARTICLE{Ueda:842465,
      author       = {Ueda, Satoru and Koizumi, Satoshi and Ohira, Akihiro and
                      Kuroda, Seiichi and Frielinghaus, Henrich},
      title        = {{G}razing-incident neutron scattering to access catalyst
                      for polymer electrolyte fuel cell},
      journal      = {Physica / B},
      volume       = {551},
      issn         = {0921-4526},
      address      = {Amsterdam},
      publisher    = {Elsevier},
      reportid     = {FZJ-2018-00699},
      pages        = {309-314},
      year         = {2018},
      abstract     = {To observe details of three phase contact in a fuel cell
                      catalyst layer and water distribution, we performed grazing
                      incidence small-angle neutron scattering (GISANS) and
                      neutron reflectivity (NR). We prepared a model catalyst on
                      silicon(Si) substrates on which platinum(Pt) and Nafion thin
                      layers are stacked. We employed two machines(KWS-1 and
                      iMATERIA, respectively), which are monochromatic at FRM-II
                      Germany and time-of-flight at J-PARC Japan. In case of Pt
                      flat surface, which was prepared by sputtering, the
                      influence due to humidification was observed in the vertical
                      direction; a water layer could be confirmed between the Pt
                      layer and the Nafion layer,increase in the thickness of the
                      Nafion layer and increase in the water content of Nafion
                      thin layer could be confirmed. The horizontal direction, on
                      the other hand, water channels (microphase separation of
                      Nafion) could not be observed in the core of thin Nafion
                      layer. We also prepared the specimen, first Pt
                      nano-particles areimplanted in a surface of Si substrate and
                      second Nafion thin layer covers by spin coating.},
      cin          = {JCNS-FRM-II / Neutronenstreuung ; JCNS-1},
      ddc          = {530},
      cid          = {I:(DE-Juel1)JCNS-FRM-II-20110218 /
                      I:(DE-Juel1)JCNS-1-20110106},
      pnm          = {6G4 - Jülich Centre for Neutron Research (JCNS) (POF3-623)
                      / 6G15 - FRM II / MLZ (POF3-6G15)},
      pid          = {G:(DE-HGF)POF3-6G4 / G:(DE-HGF)POF3-6G15},
      experiment   = {EXP:(DE-MLZ)KWS1-20140101},
      typ          = {PUB:(DE-HGF)16},
      UT           = {WOS:000455012800063},
      doi          = {10.1016/j.physb.2017.12.061},
      url          = {https://juser.fz-juelich.de/record/842465},
}