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| Hauptseite > Publikationsdatenbank > Chemical Vapor Deposition of Al 13 Fe 4 Highly Selective Catalytic Films for the Semi-Hydrogenation of Acetylene > print |
| Hauptseite > Publikationsdatenbank > Chemical Vapor Deposition of Al 13 Fe 4 Highly Selective Catalytic Films for the Semi-Hydrogenation of Acetylene > print |
| 001 | 842570 | ||
| 005 | 20210129232358.0 | ||
| 024 | 7 | _ | |a 10.1002/pssa.201700692 |2 doi |
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| 100 | 1 | _ | |a Aviziotis, Ioannis G. |0 0000-0001-5769-0768 |b 0 |
| 245 | _ | _ | |a Chemical Vapor Deposition of Al 13 Fe 4 Highly Selective Catalytic Films for the Semi-Hydrogenation of Acetylene |
| 260 | _ | _ | |a Weinheim |c 2018 |b Wiley-VCH |
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| 520 | _ | _ | |a Catalytic properties of coatings containing the Al13Fe4 intermetallic phase are tested in the reaction of semi-hydrogenation of acetylene. The selectivity to ethylene is found as high as 74% close to the reported values for pure, unsupported Al13Fe4. The initial conversion of acetylene to ethylene is 84% and rapidly drops due to the catalytic formation of carbon-based by-products on secondary Al-Fe phases. Coatings are processed through sequential chemical vapor deposition (CVD) of aluminum (5 Torr, 180 °C) and iron (40 Torr, 140 °C) layers, followed by in situ annealing for 60 min at 575 °C. Deposition proceeds at high growth rate, resulting in 15 μm thick films. After annealing, coatings are composed of the Al13Fe4 phase, co-existing with minor secondary Al-Fe intermetallic phases. Overall, it is shown that films containing complex Al-Fe intermetallic phases can be processed by CVD, opening new routes to the engineering of pure, supported Al13Fe4 catalysts on 3D or porous supports. |
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