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@ARTICLE{Liu:843618,
author = {Liu, Yi and Li, Feng and van Casteren, IIse and Tennebroe,
Ronald and Lang, Peter R.},
title = {{S}elf-, co-organisation behaviour and encapsulation
efficiency of waterborne polyurethane pre–polymers},
journal = {Colloids and surfaces / A},
volume = {544},
issn = {0927-7757},
address = {Amsterdam [u.a.]},
publisher = {Elsevier Science},
reportid = {FZJ-2018-01200},
pages = {165-171},
year = {2018},
abstract = {Polyurethane-prepolymers are the precursor for waterborne
polyurethane coating applications. The physical–chemical
behavior of the pre-polymers are worth thorough
investigation, since they will largely influence the final
properties of coating products [1–3]. In this paper, we
experimentally studied the self-, co-organization
characteristics and encapsulation efficiency of a
polyurethane pre-polymer in aqueous electrolyte environment,
by means of light scattering and small angle X-ray
scattering. Due to the amphiphilic nature, pre-polymers are
expected to form micelles in water. Systematic studies were
conducted on dispersions at different pre-polymer
concentrations and salt concentrations. Our experiments show
that the micelles have a radius of about 10 nm and are
stable over a broad range of salt concentrations; only at
high salt, 100 mM NaCl, we observe the onset of colloidal
instability. Moreover, we find that the amphiphilic
pre-polymers are able to encapsulate hydrophobic
counterparts, forming particles with radii of about
130 nm. The threshold ratio of hydrophilic over
hydrophobic pre-polymers to form stable dispersion is found
to be 5:1.},
cin = {ICS-3},
ddc = {540},
cid = {I:(DE-Juel1)ICS-3-20110106},
pnm = {551 - Functional Macromolecules and Complexes (POF3-551) /
SOMATAI - Soft Matter at Aqueous Interfaces (316866)},
pid = {G:(DE-HGF)POF3-551 / G:(EU-Grant)316866},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000428257100021},
doi = {10.1016/j.colsurfa.2018.01.052},
url = {https://juser.fz-juelich.de/record/843618},
}