% IMPORTANT: The following is UTF-8 encoded. This means that in the presence
% of non-ASCII characters, it will not work with BibTeX 0.99 or older.
% Instead, you should use an up-to-date BibTeX implementation like “bibtex8” or
% “biber”.
@ARTICLE{Dyakonova:843895,
author = {Dyakonova, Margarita A. and Gotzamanis, George and Niebuur,
Bart-Jan and Vishnevetskaya, Natalya S. and Raftopoulos,
Konstantinos N. and Di, Zhenyu and Filippov, Sergey K. and
Tsitsilianis, Constantinos and Papadakis, Christine M.},
title = {p{H} {R}esponsiveness of hydrogels formed by telechelic
polyampholytes},
journal = {Soft matter},
volume = {13},
number = {19},
issn = {1744-6848},
address = {London},
publisher = {Royal Soc. of Chemistry},
reportid = {FZJ-2018-01422},
pages = {3568 - 3579},
year = {2017},
abstract = {We investigate the influence of pH on the rheological and
structural properties of hydrogels formed by hydrophobic
association of the sticky ends of the triblock terpolymer
poly(methyl methacrylate)-b-poly(2-(diethylamino)ethyl
methacrylate-co-methacrylic acid)-b-poly(methyl
methacrylate) (PMMA-b-P(DEA-co-MAA)-b-PMMA). The middle
block is a weak polyampholyte having a pH dependent charge
density and sign, which enables tuning of the rheological
and structural properties by pH variation. Small-angle
neutron scattering (SANS) studies of solutions in D2O at
0.05 $wt\%$ and pH 3.0 reveal clusters of interconnected
spherical micelles having PMMA cores, stabilized by
repulsive ionic interactions in the middle polyampholyte
block. With increasing pH, the degree of ionization of the
DEA units decreases, whereas the one of the MAA units
increases, resulting in a complete loss of the correlation
between these micelles. At a concentration of 3 $wt\%$ at
low pH values, the system forms a gel with charged fuzzy
spheres from PMMA interacting via a screened Coulomb
potential. With increasing pH, the gel disintegrates due to
the decrease in the effective charge on the micelles. At
both concentrations, the hydrophobic aggregation of micelles
is observed near the isoelectric point. At pH 3.0–7.4, the
autocorrelation functions measured by rotational dynamic
light scattering at 3 $wt\%$ exhibit a decay steeper than
single exponential, which confirms that the gels are frozen,
presumably due to the glassy PMMA cores and hydrophobic
interpolyelectrolyte complexes. At pH 11, the diffusion of
single micelles is observed in addition to the frozen
dynamics.},
cin = {JCNS (München) ; Jülich Centre for Neutron Science JCNS
(München) ; JCNS-FRM-II / Neutronenstreuung ; JCNS-1},
ddc = {530},
cid = {I:(DE-Juel1)JCNS-FRM-II-20110218 /
I:(DE-Juel1)JCNS-1-20110106},
pnm = {6G15 - FRM II / MLZ (POF3-6G15) / 6G4 - Jülich Centre for
Neutron Research (JCNS) (POF3-623)},
pid = {G:(DE-HGF)POF3-6G15 / G:(DE-HGF)POF3-6G4},
experiment = {EXP:(DE-MLZ)KWS1-20140101},
typ = {PUB:(DE-HGF)16},
pubmed = {pmid:28443918},
UT = {WOS:000401620300012},
doi = {10.1039/C7SM00315C},
url = {https://juser.fz-juelich.de/record/843895},
}