000845361 001__ 845361
000845361 005__ 20240708132930.0
000845361 0247_ $$2doi$$a10.1063/1.5036817
000845361 0247_ $$2ISSN$$a0034-6748
000845361 0247_ $$2ISSN$$a1089-7623
000845361 0247_ $$2ISSN$$a1527-2400
000845361 0247_ $$2Handle$$a2128/19860
000845361 0247_ $$2pmid$$apmid:30184627
000845361 0247_ $$2WOS$$aWOS:000443720400003
000845361 037__ $$aFZJ-2018-02635
000845361 082__ $$a530
000845361 1001_ $$0P:(DE-Juel1)166215$$aScheepers, Fabian$$b0$$eCorresponding author
000845361 245__ $$aA New Setup for the Quantitive Analysis of Drying by the Use of Gas-phase FTIR-Spectroscopy
000845361 260__ $$a[S.l.]$$bAmerican Institute of Physics$$c2018
000845361 3367_ $$2DRIVER$$aarticle
000845361 3367_ $$2DataCite$$aOutput Types/Journal article
000845361 3367_ $$0PUB:(DE-HGF)16$$2PUB:(DE-HGF)$$aJournal Article$$bjournal$$mjournal$$s1540387593_3258
000845361 3367_ $$2BibTeX$$aARTICLE
000845361 3367_ $$2ORCID$$aJOURNAL_ARTICLE
000845361 3367_ $$00$$2EndNote$$aJournal Article
000845361 520__ $$aDrying rates are important for the manufacture of thin films and in specific for the production of electrodes used in electrochemical devices such as fuel cells and electrolyzers. The known procedures to investigate time-dependent sample compositions and selective evaporation rates are insufficient to obtain mean information about the full area instead of a single point analysis. Therefore, a new setup is presented using gas-phase Fourier-transform infrared spectroscopy. This method analyzes the gas-phase composition to recalculate the layer composition in electrode fabrication at any time during drying. According to the golden rule of measurement technology, manufacturer specifications are often overestimated. Therefore, our alternative procedures were used to evaluate the precision of devices used. The calculated measurement precision is confirmed by validation. The expected deviation is quantified to be less than 2% for the common application. Further on, the relative test-retest standard deviation is determined to be 0.3%–0.4%. As a result of the error propagation, the measurement precision is limited by the background gas flow rate precision for common application. At low volume fractions, the influence of the substance flow rate deviations becomes significant. However, further studies will focus on increasing the gas flow rate precision
000845361 536__ $$0G:(DE-HGF)POF3-135$$a135 - Fuel Cells (POF3-135)$$cPOF3-135$$fPOF III$$x0
000845361 588__ $$aDataset connected to CrossRef
000845361 7001_ $$0P:(DE-Juel1)132718$$aBurdzik, Andrea$$b1
000845361 7001_ $$0P:(DE-Juel1)129930$$aStähler, Markus$$b2
000845361 7001_ $$0P:(DE-Juel1)145276$$aCarmo, Marcelo$$b3
000845361 7001_ $$0P:(DE-Juel1)129883$$aLehnert, Werner$$b4
000845361 7001_ $$0P:(DE-Juel1)129928$$aStolten, Detlef$$b5
000845361 773__ $$0PERI:(DE-600)1472905-2$$a10.1063/1.5036817$$gVol. 89, no. 8, p. 083102 -$$n8$$p083102 -$$tReview of scientific instruments$$v89$$x0034-6748$$y2018
000845361 8564_ $$uhttps://juser.fz-juelich.de/record/845361/files/1.5036817.pdf$$yPublished on 2018-08-03. Available in OpenAccess from 2019-08-03.
000845361 8564_ $$uhttps://juser.fz-juelich.de/record/845361/files/1.5036817.pdf?subformat=pdfa$$xpdfa$$yPublished on 2018-08-03. Available in OpenAccess from 2019-08-03.
000845361 909CO $$ooai:juser.fz-juelich.de:845361$$pdnbdelivery$$pdriver$$pVDB$$popen_access$$popenaire
000845361 9101_ $$0I:(DE-588b)5008462-8$$6P:(DE-Juel1)166215$$aForschungszentrum Jülich$$b0$$kFZJ
000845361 9101_ $$0I:(DE-588b)5008462-8$$6P:(DE-Juel1)132718$$aForschungszentrum Jülich$$b1$$kFZJ
000845361 9101_ $$0I:(DE-588b)5008462-8$$6P:(DE-Juel1)129930$$aForschungszentrum Jülich$$b2$$kFZJ
000845361 9101_ $$0I:(DE-588b)5008462-8$$6P:(DE-Juel1)145276$$aForschungszentrum Jülich$$b3$$kFZJ
000845361 9101_ $$0I:(DE-588b)5008462-8$$6P:(DE-Juel1)129883$$aForschungszentrum Jülich$$b4$$kFZJ
000845361 9101_ $$0I:(DE-588b)36225-6$$6P:(DE-Juel1)129883$$aRWTH Aachen$$b4$$kRWTH
000845361 9101_ $$0I:(DE-588b)5008462-8$$6P:(DE-Juel1)129928$$aForschungszentrum Jülich$$b5$$kFZJ
000845361 9101_ $$0I:(DE-588b)36225-6$$6P:(DE-Juel1)129928$$aRWTH Aachen$$b5$$kRWTH
000845361 9131_ $$0G:(DE-HGF)POF3-135$$1G:(DE-HGF)POF3-130$$2G:(DE-HGF)POF3-100$$3G:(DE-HGF)POF3$$4G:(DE-HGF)POF$$aDE-HGF$$bEnergie$$lSpeicher und vernetzte Infrastrukturen$$vFuel Cells$$x0
000845361 9141_ $$y2018
000845361 915__ $$0StatID:(DE-HGF)0200$$2StatID$$aDBCoverage$$bSCOPUS
000845361 915__ $$0StatID:(DE-HGF)1160$$2StatID$$aDBCoverage$$bCurrent Contents - Engineering, Computing and Technology
000845361 915__ $$0StatID:(DE-HGF)0600$$2StatID$$aDBCoverage$$bEbsco Academic Search
000845361 915__ $$0StatID:(DE-HGF)0530$$2StatID$$aEmbargoed OpenAccess
000845361 915__ $$0StatID:(DE-HGF)0100$$2StatID$$aJCR$$bREV SCI INSTRUM : 2015
000845361 915__ $$0StatID:(DE-HGF)0150$$2StatID$$aDBCoverage$$bWeb of Science Core Collection
000845361 915__ $$0StatID:(DE-HGF)0110$$2StatID$$aWoS$$bScience Citation Index
000845361 915__ $$0StatID:(DE-HGF)0111$$2StatID$$aWoS$$bScience Citation Index Expanded
000845361 915__ $$0StatID:(DE-HGF)9900$$2StatID$$aIF < 5
000845361 915__ $$0StatID:(DE-HGF)0030$$2StatID$$aPeer Review$$bASC
000845361 915__ $$0StatID:(DE-HGF)1150$$2StatID$$aDBCoverage$$bCurrent Contents - Physical, Chemical and Earth Sciences
000845361 915__ $$0StatID:(DE-HGF)0300$$2StatID$$aDBCoverage$$bMedline
000845361 915__ $$0StatID:(DE-HGF)0420$$2StatID$$aNationallizenz
000845361 915__ $$0StatID:(DE-HGF)0199$$2StatID$$aDBCoverage$$bThomson Reuters Master Journal List
000845361 920__ $$lyes
000845361 9201_ $$0I:(DE-Juel1)IEK-3-20101013$$kIEK-3$$lElektrochemische Verfahrenstechnik$$x0
000845361 9801_ $$aFullTexts
000845361 980__ $$ajournal
000845361 980__ $$aVDB
000845361 980__ $$aUNRESTRICTED
000845361 980__ $$aI:(DE-Juel1)IEK-3-20101013
000845361 981__ $$aI:(DE-Juel1)ICE-2-20101013