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@ARTICLE{Schmitz:845649,
author = {Schmitz, Paulo and Kolek, Martin and Diddens, Diddo and
Stan, Marian Cristian and Jalkanen, Kirsi and Winter, Martin
and Bieker, Peter},
title = {{C}ounterintuitive trends of the wetting behavior of ionic
liquid-based electrolytes on modified lithium electrodes},
journal = {Physical chemistry, chemical physics},
volume = {19},
number = {29},
issn = {1463-9084},
address = {Cambridge},
publisher = {RSC Publ.},
reportid = {FZJ-2018-02865},
pages = {19178 - 19187},
year = {2017},
abstract = {The demand for high energy densities has brought
rechargeable lithium metal batteries back into the research
focus. Ionic liquids (ILs) are considered as suitable
electrolyte components for these systems. In this work, the
wetting behavior of 1-ethyl-3-methylimidazolium
bis((trifluoromethyl)sulfonyl)imide ([C2MIm]TFSI),
1-butyl-3-methylimidazolium
bis-((trifluoromethyl)sulfonyl)imide ([C4MIm]TFSI),
1-hexyl-3-methylimidazolium
bis((trifluoromethyl)sulfonyl)imide ([C6MIm]TFSI), and
N-butyl-N-methylpyrrolidinium
bis((trifluoromethyl)sulfonyl)imide (Pyr14TFSI) on
mechanically modified lithium electrodes, with and without
lithium bis((trifluoromethyl)sulfonyl)imide (LiTFSI)
conducting salt, is investigated and is compared to an
organic carbonate-based electrolyte. Three different
patterns were chosen for the lithium modification, enabling
a surface area increase of $12\%,$ $20\%,$ and $56\%$ for
the modified lithium electrodes. Especially for pure ILs,
the contact angle on lithium was significantly larger with
higher surface areas of the lithium electrodes. Since the
addition of LiTFSI remarkably decreased the contact angles
of the ILs on the modified lithium surfaces, it could be
shown that the effect of LiTFSI can be attributed to a
decreased surface tension. This observation could be
explained by an interruption of the ordering of ionic liquid
cations and anions, which is supported by Raman spectroscopy
and molecular dynamics (MD) simulations.},
cin = {IEK-12},
ddc = {540},
cid = {I:(DE-Juel1)IEK-12-20141217},
pnm = {131 - Electrochemical Storage (POF3-131)},
pid = {G:(DE-HGF)POF3-131},
typ = {PUB:(DE-HGF)16},
pubmed = {pmid:28702548},
UT = {WOS:000406334300037},
doi = {10.1039/C7CP03716C},
url = {https://juser.fz-juelich.de/record/845649},
}