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@ARTICLE{Hufnagel:848218,
author = {Hufnagel, Alexander and Ann‐Kathrin Henß and Hoffmann,
Ramona and Zeman, Otto and Häringer, Sebastian and
Fattakhova-Rohlfing, Dina and Bein, Thomas},
title = {{E}lectron‐{B}locking and {O}xygen {E}volution {C}atalyst
{L}ayers by {P}lasma‐{E}nhanced {A}tomic {L}ayer
{D}eposition of {N}ickel {O}xide},
journal = {Advanced materials interfaces},
volume = {5},
number = {16},
issn = {2196-7350},
address = {Weinheim},
publisher = {Wiley-VCH},
reportid = {FZJ-2018-03480},
pages = {1701531},
year = {2018},
abstract = {A plasma‐enhanced atomic layer deposition (ALD) process
is presented, capable of producing thin conformal films of
nickel(II) oxide (NiO) on various substrates. Nickelocene
(NiCp2) is used as an inexpensive metal precursor with
oxygen plasma as the oxidant. The film growth rate saturates
with both nickel precursor and plasma exposure. An ALD
window is observed between 225 and 275 °C. Linear growth is
achieved at 250 °C with a growth rate of 0.042 nm per
cycle. The thickness is highly uniform and the surface
roughness is below 1 nm rms for 52 nm thick films on
Si(100). Substrates with aspect ratios up to 1:10 can be
processed. As‐deposited, the films consist of
polycrystalline, cubic NiO, and are transparent over the
entire visible range with an optical bandgap of 3.7 eV. The
films consist of stoichiometric NiO and contain $≈1\%$ of
carbon impurities. Two promising applications of these films
are showcased in renewable energy conversion and storage
devices: The films are pinhole‐free and exhibit excellent
electron blocking capabilities, making them potential
hole‐selective contact layers in solar cells. Also, high
electrocatalytic activity of ultrathin NiO films is
demonstrated for the alkaline oxygen evolution reaction,
especially in electrolytes containing Fe3+.},
cin = {IEK-1},
ddc = {540},
cid = {I:(DE-Juel1)IEK-1-20101013},
pnm = {899 - ohne Topic (POF3-899)},
pid = {G:(DE-HGF)POF3-899},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000442489600001},
doi = {10.1002/admi.201701531},
url = {https://juser.fz-juelich.de/record/848218},
}