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@ARTICLE{Rodenbcher:848464,
author = {Rodenbücher, C. and Bihlmayer, G. and Speier, W. and
Kubacki, J. and Wojtyniak, M. and Rogala, M. and Wrana, D.
and Krok, F. and Szot, K.},
title = {{L}ocal surface conductivity of transition metal oxides
mapped with true atomic resolution},
journal = {Nanoscale},
volume = {10},
number = {24},
issn = {2040-3372},
address = {Cambridge},
publisher = {RSC Publ.},
reportid = {FZJ-2018-03698},
pages = {11498 - 11505},
year = {2018},
abstract = {The introduction of transition metal oxides for building
nanodevices in information technology promises to overcome
the scaling limits of conventional semiconductors and to
reduce global power consumption significantly. However,
oxide surfaces can exhibit heterogeneity on the nanoscale
e.g. due to relaxation, rumpling, reconstruction, or
chemical variations which demands for direct
characterization of electronic transport phenomena down to
the atomic level. Here we demonstrate that conductivity
mapping is possible with true atomic resolution using the
tip of a local conductivity atomic force microscope (LC-AFM)
as the mobile nanoelectrode. The application to the
prototypical transition metal oxide TiO2 self-doped by
oxygen vacancies reveals the existence of highly confined
current paths in the first stage of thermal reduction.
Assisted by density functional theory (DFT) we propose that
the presence of oxygen vacancies in the surface layer of
such materials can introduce short range disturbances of the
electronic structure with confinement of metallic states on
the sub-nanometre scale. After prolonged reduction, the
surfaces undergo reconstruction and the conductivity changes
from spot-like to homogeneous as a result of surface
transformation. The periodic arrangement of the
reconstruction is clearly reflected in the conductivity maps
as concluded from the simultaneous friction force and LC-AFM
measurements. The second prototype metal oxide SrTiO3 also
reveals a comparable transformation in surface conductivity
from spot-like to homogeneous upon reduction showing the
relevance of nanoscale inhomogeneities for the electronic
transport properties and the utility of a high-resolution
LC-AFM as a convenient tool to detect them.},
cin = {PGI-7 / PGI-1 / IAS-1 / JARA-FIT / JARA-HPC},
ddc = {600},
cid = {I:(DE-Juel1)PGI-7-20110106 / I:(DE-Juel1)PGI-1-20110106 /
I:(DE-Juel1)IAS-1-20090406 / $I:(DE-82)080009_20140620$ /
$I:(DE-82)080012_20140620$},
pnm = {142 - Controlling Spin-Based Phenomena (POF3-142) /
Magnetic Anisotropy of Metallic Layered Systems and
Nanostructures $(jiff13_20131101)$},
pid = {G:(DE-HGF)POF3-142 / $G:(DE-Juel1)jiff13_20131101$},
typ = {PUB:(DE-HGF)16},
pubmed = {pmid:29888770},
UT = {WOS:000436133400031},
doi = {10.1039/C8NR02562B},
url = {https://juser.fz-juelich.de/record/848464},
}