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@ARTICLE{Escolstico:849644,
author = {Escolástico, S. and Stournari, V. and Malzbender, J. and
Haas-Santo, K. and Dittmeyer, R. and Serra, J. M.},
title = {{C}hemical stability in {H} 2 {S} and creep
characterization of the mixed protonic conductor {N}d 5.5
{WO} 11.25-δ},
journal = {International journal of hydrogen energy},
volume = {43},
number = {17},
issn = {0360-3199},
address = {New York, NY [u.a.]},
publisher = {Elsevier},
reportid = {FZJ-2018-03785},
pages = {8342 - 8354},
year = {2018},
abstract = {The integration of hydrogen permeable membranes in
catalytic membrane reactors for thermodynamically limited
reactions such as steam methane reforming can improve the
per-pass yield and simultaneously produce a high-purity H2
stream. Mixed protonic-electronic materials based membranes
are potential candidates for these applications due to their
elevated temperature operation, good stability and
potentially low cost. However, a specific mechanical
behavior and stability under harsh atmospheres is needed to
guarantee sufficient lifetime in real-world processes. This
work presents the mechanical characterization and a study of
the chemical stability under H2S containing atmospheres for
the compound Nd5.5WO11.25-δ. Mechanical characterization
was performed by micro-indentation and creep measurements in
air. Chemical stability was evaluated by XRD and SEM and the
effect of the H2S on the transport properties was evaluated
by impedance spectroscopy. Under H2S atmospheres, the total
conductivity increases at 600 °C and 700 °C. The
conductivity increase is attributed to the incorporation of
S2− ions in oxide-ion sublattice.},
cin = {IEK-2},
ddc = {660},
cid = {I:(DE-Juel1)IEK-2-20101013},
pnm = {111 - Efficient and Flexible Power Plants (POF3-111)},
pid = {G:(DE-HGF)POF3-111},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000431747600016},
doi = {10.1016/j.ijhydene.2018.03.060},
url = {https://juser.fz-juelich.de/record/849644},
}