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@PHDTHESIS{Thaler:850283,
author = {Thaler, Florian},
title = {{D}er {E}influss von {W}asserdampf auf den
{S}auerstofftransport in keramischen
{H}ochtemperaturmembranen},
volume = {430},
school = {RWTH Aachen},
type = {Dissertation},
address = {Jülich},
publisher = {Forschungszentrum Jülich GmbH Zentralbibliothek, Verlag},
reportid = {FZJ-2018-04325},
isbn = {978-3-95806-340-2},
series = {Schriften des Forschungszentrums Jülich Reihe Energie $\&$
Umwelt / Energy $\&$ Environment},
pages = {ii, 93, XXXI S.},
year = {2018},
note = {RWTH Aachen, Diss., 2018},
abstract = {Ceramic high temperature oxygen transport membranes (OTMs)
represent a promising alternative for the extraction of
oxygen from ambient air compared to conventional high-energy
intensive processes like cryogenic air separation.
Especially materials with a mixed ionic and electronic
conductivity (MIEC) are of current interest as O$^{2-}$-ion
conductors. The high number of vacancies and the high
mobility for electrons at sufficient high temperature and
partial pressure gradient, enables these materials to
transport oxygen via the crystal lattice and achieve a 100\%
selectivity. Due to their high conductivities, mostly
perovskites or a combination of fluorite- and spinel-phases
are used as OTM-materials. Depending on the application,
OTMs can be used either directly for the oxygen production
or in a so-called membrane reactor where chemical reactions
are controlled by selective oxidation of particular
reactants. This work examines the so-called
"oxyfuel-combustion", where fossil fuels like coal are
combusted under pure oxygen atmosphere in a power plant, to
reduce NOx-emissions and make the combustion more efficient.
A OTM-module implemented in the power plant should provide
the needed amount of oxygen. The flue gas of such a oxyfuel
power plant consist, except for H$_{2}$O and traces of
SO$_{2}$, of a pure CO$_{2}$-stream which can be directly
used for Carbon Dioxide Capture and Storage. To reduce the
high temperatures occurring in the oxyfuel-combustion and to
flush the oxygen from the membrane module, usually recycled
flue gas is used. Unfortunately some of the most promising
OTMmaterials show degradations facing CO2 and CO from the
flue gas. Therefore a new concept was invented, where water
vapor is used to sweep the membrane instead of the
aggressive flue gas. On this point the current work deals
with lab-scale experiments on different membrane materials
in a permeation measurement setup with humidied sweep gas.
Several OTM-materials are investigated concerning their
long-term stability and the degradation of the permeation
performance while using different amounts of water vapor in
the sweep. All tested materials show a decreasing permeation
rate for oxygen with increasing water content. The reason
for this declined performance can be explained by
miscellaneous materials corrosion and degradation
mechanisms, which are discussed in the results part.},
cin = {IEK-2},
cid = {I:(DE-Juel1)IEK-2-20101013},
pnm = {899 - ohne Topic (POF3-899)},
pid = {G:(DE-HGF)POF3-899},
typ = {PUB:(DE-HGF)3 / PUB:(DE-HGF)11},
url = {https://juser.fz-juelich.de/record/850283},
}