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@INPROCEEDINGS{Ma:851085,
author = {Ma, Qianli and Tsai, Chih-Long and Tietz, Frank},
title = {{A} room-temperature full-ceramic sodium-ion battery based
on {N}a3+x{Z}r2{S}i2+x{P}1-x{O}12 as sodium superionic
conductor},
reportid = {FZJ-2018-04793},
year = {2018},
abstract = {Despite of huge efforts, the lack of suitable candidate for
electrolytes still impedes the development of
all-solid-state Na batteries. Na3+xZr2Si2+xP1-xO12 (-0.2 ≤
x ≤ 0.2) are the very first composition series of NASICONs
discovered 40 years ago and were reported having a total
Na-ion conductivity of ~10-4 S cm-1 at room temperature. In
the present study, this composition series is reconsidered
and the focusing range of stoichiometry has been varied from
x = 0 to x = 0.6. A solution-assisted solid-state reaction
method is applied for powder preparation. Surprisingly, a
total conductivity of over 5 × 10-3 S cm-1 is achieved for
Na3.4Zr2Si2.4P0.6O12 at 25 °C, which is the best value of
all reported polycrystalline Na-ion conductors. A bulk
conductivity of about 1.5 × 10-2 S cm-1 is also revealed by
high frequency impedance spectroscopy up to 3 GHz for
Na3.4Zr2Si2.4P0.6O12 at 25 °C. The parameters influencing
the total conductivity are discussed in detail. Benefitted
from the superior total conductivity of
Na3.4Zr2Si2.4P0.6O12, a full-ceramic cell has been
fabricated and tested at 28 °C with good cycling
performance. To our knowledge, this is the first full
ceramic Na-ion battery which has been operated at room
temperature.},
month = {Jul},
date = {2018-07-22},
organization = {12th International Conference on
Ceramic Materials and Components for
Energy and Environmental Applications,
Singapore (Singapore), 22 Jul 2018 - 27
Jul 2018},
subtyp = {Invited},
cin = {IEK-1},
cid = {I:(DE-Juel1)IEK-1-20101013},
pnm = {131 - Electrochemical Storage (POF3-131) / SOFC - Solid
Oxide Fuel Cell (SOFC-20140602)},
pid = {G:(DE-HGF)POF3-131 / G:(DE-Juel1)SOFC-20140602},
typ = {PUB:(DE-HGF)6},
url = {https://juser.fz-juelich.de/record/851085},
}