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000851128 1001_ $$0P:(DE-HGF)0$$aMenzel, Jennifer$$b0
000851128 245__ $$aQuantification of ionic organo(fluoro)phosphates in decomposed lithium battery electrolytes
000851128 260__ $$aLondon$$bRSC Publishing$$c2017
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000851128 520__ $$aA method for the separation, identification and quantification of the ionic decomposition products of LiPF6 based organic electrolytes was developed. It employed the simultaneous coupling of two-dimensional ion chromatography (2D IC) with electrospray-ionization mass spectrometry (ESI-MS) and with inductively coupled plasma-mass spectrometry (ICP-MS). The electrolyte under investigation was a commercially available electrolyte by BASF, consisting of 1 mol L−1 LiPF6 in a mixture of one linear and one cyclic organic carbonate (50[thin space (1/6-em)]:[thin space (1/6-em)]50 wt%). The quantification was based on the use of a structurally similar compound as calibration standard for the ICP-MS measurement, while the identification was carried out with ESI-MS. Several organo(fluoro)phosphate species were successfully separated and quantified. Since these species show a high structural similarity to the warfare agent sarin, their investigation is of special interest with regard to their potential toxicity. Additionally, a quantification study of an electrolyte extracted from a cycled lithium metal cell was carried out.
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000851128 7001_ $$0P:(DE-HGF)0$$aSchultz, Hannah$$b1
000851128 7001_ $$0P:(DE-HGF)0$$aKraft, Vadim$$b2
000851128 7001_ $$0P:(DE-HGF)0$$aBadillo, Juan Pablo$$b3
000851128 7001_ $$0P:(DE-Juel1)166130$$aWinter, Martin$$b4$$ufzj
000851128 7001_ $$00000-0003-1508-6073$$aNowak, Sascha$$b5$$eCorresponding author
000851128 773__ $$0PERI:(DE-600)2623224-8$$a10.1039/C7RA07486G$$gVol. 7, no. 62, p. 39314 - 39324$$n62$$p39314 - 39324$$tRSC Advances$$v7$$x2046-2069$$y2017
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