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@ARTICLE{Menzel:851128,
      author       = {Menzel, Jennifer and Schultz, Hannah and Kraft, Vadim and
                      Badillo, Juan Pablo and Winter, Martin and Nowak, Sascha},
      title        = {{Q}uantification of ionic organo(fluoro)phosphates in
                      decomposed lithium battery electrolytes},
      journal      = {RSC Advances},
      volume       = {7},
      number       = {62},
      issn         = {2046-2069},
      address      = {London},
      publisher    = {RSC Publishing},
      reportid     = {FZJ-2018-04830},
      pages        = {39314 - 39324},
      year         = {2017},
      abstract     = {A method for the separation, identification and
                      quantification of the ionic decomposition products of LiPF6
                      based organic electrolytes was developed. It employed the
                      simultaneous coupling of two-dimensional ion chromatography
                      (2D IC) with electrospray-ionization mass spectrometry
                      (ESI-MS) and with inductively coupled plasma-mass
                      spectrometry (ICP-MS). The electrolyte under investigation
                      was a commercially available electrolyte by BASF, consisting
                      of 1 mol L−1 LiPF6 in a mixture of one linear and one
                      cyclic organic carbonate (50[thin space (1/6-em)]:[thin
                      space (1/6-em)]50 $wt\%).$ The quantification was based on
                      the use of a structurally similar compound as calibration
                      standard for the ICP-MS measurement, while the
                      identification was carried out with ESI-MS. Several
                      organo(fluoro)phosphate species were successfully separated
                      and quantified. Since these species show a high structural
                      similarity to the warfare agent sarin, their investigation
                      is of special interest with regard to their potential
                      toxicity. Additionally, a quantification study of an
                      electrolyte extracted from a cycled lithium metal cell was
                      carried out.},
      cin          = {IEK-12},
      ddc          = {540},
      cid          = {I:(DE-Juel1)IEK-12-20141217},
      pnm          = {131 - Electrochemical Storage (POF3-131)},
      pid          = {G:(DE-HGF)POF3-131},
      typ          = {PUB:(DE-HGF)16},
      UT           = {WOS:000407762300067},
      doi          = {10.1039/C7RA07486G},
      url          = {https://juser.fz-juelich.de/record/851128},
}