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| Hauptseite > Publikationsdatenbank > Quantification of ionic organo(fluoro)phosphates in decomposed lithium battery electrolytes > print |
| Hauptseite > Publikationsdatenbank > Quantification of ionic organo(fluoro)phosphates in decomposed lithium battery electrolytes > print |
| 001 | 851128 | ||
| 005 | 20240712113116.0 | ||
| 024 | 7 | _ | |a 10.1039/C7RA07486G |2 doi |
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| 037 | _ | _ | |a FZJ-2018-04830 |
| 082 | _ | _ | |a 540 |
| 100 | 1 | _ | |a Menzel, Jennifer |0 P:(DE-HGF)0 |b 0 |
| 245 | _ | _ | |a Quantification of ionic organo(fluoro)phosphates in decomposed lithium battery electrolytes |
| 260 | _ | _ | |a London |c 2017 |b RSC Publishing |
| 336 | 7 | _ | |a article |2 DRIVER |
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| 336 | 7 | _ | |a Journal Article |0 0 |2 EndNote |
| 520 | _ | _ | |a A method for the separation, identification and quantification of the ionic decomposition products of LiPF6 based organic electrolytes was developed. It employed the simultaneous coupling of two-dimensional ion chromatography (2D IC) with electrospray-ionization mass spectrometry (ESI-MS) and with inductively coupled plasma-mass spectrometry (ICP-MS). The electrolyte under investigation was a commercially available electrolyte by BASF, consisting of 1 mol L−1 LiPF6 in a mixture of one linear and one cyclic organic carbonate (50[thin space (1/6-em)]:[thin space (1/6-em)]50 wt%). The quantification was based on the use of a structurally similar compound as calibration standard for the ICP-MS measurement, while the identification was carried out with ESI-MS. Several organo(fluoro)phosphate species were successfully separated and quantified. Since these species show a high structural similarity to the warfare agent sarin, their investigation is of special interest with regard to their potential toxicity. Additionally, a quantification study of an electrolyte extracted from a cycled lithium metal cell was carried out. |
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| 700 | 1 | _ | |a Schultz, Hannah |0 P:(DE-HGF)0 |b 1 |
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| 700 | 1 | _ | |a Badillo, Juan Pablo |0 P:(DE-HGF)0 |b 3 |
| 700 | 1 | _ | |a Winter, Martin |0 P:(DE-Juel1)166130 |b 4 |u fzj |
| 700 | 1 | _ | |a Nowak, Sascha |0 0000-0003-1508-6073 |b 5 |e Corresponding author |
| 773 | _ | _ | |a 10.1039/C7RA07486G |g Vol. 7, no. 62, p. 39314 - 39324 |0 PERI:(DE-600)2623224-8 |n 62 |p 39314 - 39324 |t RSC Advances |v 7 |y 2017 |x 2046-2069 |
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