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@ARTICLE{Janssen:851136,
author = {Janssen, Pia and Streipert, Benjamin and Krafft, Roman and
Murmann, Patrick and Wagner, Ralf and Lewis-Alleyne, Lesley
and Röschenthaler, Gerd-Volker and Winter, Martin and
Cekic-Laskovic, Isidora},
title = {{S}hutdown potential adjustment of modified carbene adducts
as additives for lithium ion battery electrolytes},
journal = {Journal of power sources},
volume = {367},
issn = {0378-7753},
address = {New York, NY [u.a.]},
publisher = {Elsevier},
reportid = {FZJ-2018-04838},
pages = {72 - 79},
year = {2017},
abstract = {To improve the intrinsic safety of lithium ion batteries
(LIBs) by preventing cells from a thermal runaway, we
studied two carbene adduct electrolyte additives. The
recently synthesized compounds
(1,3-dimethylimidazolidin-2-μm-trifluoroborate (NHC-BF3)
and
1,3-dimethylimidazolidin-2-μm-tetrafluorotrifluoromethylphosphate
(NHC-PF4CF3)) were investigated on LiNi1/3Co1/3Mn1/3O2
(NMC111) electrodes in Li metal and Li-ion cell setups as
overcharge protection shutdown additives in 1M LiPF6 in
EC:DEC (3:7, by wt.) electrolyte. By varying the NHC-ligand
(-BF3, -PF5, -PF4CF3) in the molecule, the shutdown
potential of the investigated carbene adduct electrolyte
additives can be tailored for specific applications with
different cut-off potentials. NHC-BF3 was identified as a
promising candidate for the application with NMC111
electrodes up to 4.4 V vs. Li/Li+, whereas the carbene
adduct NHC-PF4CF3 is ideal for the high-voltage application
with the NMC-based electrode up to 4.6 V vs. Li/Li+. Next to
electrochemical investigations in NMC111/Li and
NMC111/graphite cells, Atomic Force Microscopy (AFM) and
X-Ray Photoelectron Spectroscopy (XPS) were performed to
verify the presence of a decomposition layer on the cathode,
responsible for the shutdown effect. Furthermore, it has
been proven that the investigated electrolyte additives have
no influence on the cell performance under normal conditions
in both, Li metal and Li-ion cell setups.},
cin = {IEK-12},
ddc = {620},
cid = {I:(DE-Juel1)IEK-12-20141217},
pnm = {131 - Electrochemical Storage (POF3-131)},
pid = {G:(DE-HGF)POF3-131},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000415780000010},
doi = {10.1016/j.jpowsour.2017.09.023},
url = {https://juser.fz-juelich.de/record/851136},
}