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@ARTICLE{Heckmann:851169,
author = {Heckmann, A and Thienenkamp, J and Beltrop, K and Winter,
Martin and Brunklaus, Gunther and Placke, T},
title = {{T}owards high-performance dual-graphite batteries using
highly concentrated organic electrolytes},
journal = {Electrochimica acta},
volume = {260},
issn = {0013-4686},
address = {New York, NY [u.a.]},
publisher = {Elsevier},
reportid = {FZJ-2018-04869},
pages = {514-525},
year = {2018},
abstract = {Dual-ion batteries (DIBs) and dual-graphite batteries
(DGBs) attract increasing attention as an alternative
approach for stationary energy storage due to their
environmental, cost and safety benefits over other
state-of-the-art battery technologies. In order to realize
an extraordinary cell performance of DGBs, it is of
particular importance to stabilize the interphases between
electrolyte and electrode, for both the negative and
positive electrodes. In this work, we present the
implementation of highly concentrated electrolytes (HCEs) in
DIBs and DGBs, i.e. electrolyte formulations based on either
LiPF6 or LiTFSI in dimethyl carbonate (DMC), diethyl
carbonate (DEC) or ethyl methyl carbonate (EMC). A
reversible cycling stability of the graphitic negative
electrode is proven as well as the stability of the HCEs
against oxidative decomposition at the positive electrode at
a cathode potential of 5V vs. Li/Li+. Additionally, we
demonstrate that the anodic dissolution of the aluminum (Al)
current collector is successfully suppressed by using
LiTFSI-based HCEs, which show a comparable resistivity
against Al dissolution as LiPF6-based electrolytes.
Furthermore, a strong dependence of concentration and onset
potential of anion intercalation is observed and
comprehensively discussed with respect to the thermodynamic
environment of the electrolyte. Overall, the use of HCEs
enables a highly reversible cycling stability, providing
extraordinary high specific discharge capacities of
80–100 mAh g−1 for lithium metal-based DIBs and DGBs.
The evaluation of voltage efficiency (VE) and energy
efficiency (EE) reveals the highest values for the
EMC/LiPF6-based electrolyte, i.e. $96\%$ (VE) and $95\%$
(EE). In summary, the use of HCEs is a promising strategy to
further optimize the electrochemical performance of DIBs and
DGBs in terms of high reversible capacity and cycling
stability and decreased parasitic side reactions.},
cin = {IEK-12},
ddc = {540},
cid = {I:(DE-Juel1)IEK-12-20141217},
pnm = {131 - Electrochemical Storage (POF3-131)},
pid = {G:(DE-HGF)POF3-131},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000419831600058},
doi = {10.1016/j.electacta.2017.12.099},
url = {https://juser.fz-juelich.de/record/851169},
}