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@ARTICLE{Beltrop:851243,
author = {Beltrop, Kolja and Klein, Sven and Nölle, Roman and
Wilken, Andrea and Lee, Juhyon J. and Köster, Thomas K.-J.
and Reiter, Jakub and Tao, Liang and Liang, Chengdu and
Winter, Martin and Qi, Xin and Placke, Tobias},
title = {{T}riphenylphosphine {O}xide as {H}ighly {E}ffective
{E}lectrolyte {A}dditive for {G}raphite/{NMC}811 {L}ithium
{I}on {C}ells},
journal = {Chemistry of materials},
volume = {30},
number = {8},
issn = {1520-5002},
address = {Washington, DC},
publisher = {American Chemical Society},
reportid = {FZJ-2018-04938},
pages = {2726 - 2741},
year = {2018},
abstract = {Nickel-rich layered oxide materials (LiNixMnyCo1–x–yO2,
x ≥ 0.8, LiNMC) attract great interest for application as
positive electrode in lithium ion batteries (LIBs) due to
high specific discharge capacities at moderate upper cutoff
voltages below 4.4 V vs Li/Li+. However, the comparatively
poor cycling stability as well as inferior safety
characteristics prevent this material class from commercial
application so far. Against this background, new electrolyte
formulations including additives are a major prerequisite
for a sufficient electrochemical performance of Ni-rich NMC
materials. In this work, we introduce triphenylphosphine
oxide (TPPO) as electrolyte additive for the application in
graphite/LiNi0.8Mn0.1Co0.1O2 (NMC811) cells. The addition of
only 0.5 wt $\%$ TPPO into a carbonate-based electrolyte
(LiPF6 in EC:EMC) significantly increases the first cycle
Coulombic efficiency as well as the reversible specific
capacity and improves the capacity retention of the LIB full
cell cycled between 2.8 and 4.3 V. Electrochemical results
indicate that the full cell capacity fade is predominantly
caused by active lithium loss at the negative electrode. In
this contribution, X-ray photoelectron spectroscopy and
inductively coupled plasma-mass spectrometry analysis
confirm the participation of the electrolyte additive in the
solid electrolyte interphase formation on the negative
electrode as well as in the cathode electrolyte interphase
formation on the positive electrode, thus, effectively
reducing the active lithium loss during cycling.
Furthermore, the performance of the TPPO additive is
compared to literature known electrolyte additives including
triphenylphosphine, vinylene carbonate, and diphenyl
carbonate demonstrating the outstanding working ability of
TPPO in graphite/NMC811 cells.},
cin = {IEK-12},
ddc = {540},
cid = {I:(DE-Juel1)IEK-12-20141217},
pnm = {131 - Electrochemical Storage (POF3-131)},
pid = {G:(DE-HGF)POF3-131},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000431088400029},
doi = {10.1021/acs.chemmater.8b00413},
url = {https://juser.fz-juelich.de/record/851243},
}