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@ARTICLE{Yu:851351,
author = {Yu, Shicheng and Mertens, Andreas and Tempel, Hermann and
Schierholz, Roland and Kungl, Hans and Eichel, Rüdiger-A.},
title = {{M}onolithic {A}ll-{P}hosphate {S}olid-{S}tate
{L}ithium-{I}on {B}attery with {I}mproved {I}nterfacial
{C}ompatibility},
journal = {ACS applied materials $\&$ interfaces},
volume = {10},
number = {26},
issn = {1944-8252},
address = {Washington, DC},
publisher = {Soc.},
reportid = {FZJ-2018-05036},
pages = {22264 - 22277},
year = {2018},
abstract = {High interfacial resistance between solid electrolyte and
electrode of ceramic all-solid-state batteries is a major
reason for the reduced performance of these batteries. A
solid-state battery using a monolithic all-phosphate concept
based on screen printed thick LiTi2(PO4)3 anode and
Li3V2(PO4)3 cathode composite layers on a densely sintered
Li1.3Al0.3Ti1.7(PO4)3 solid electrolyte has been realized
with competitive cycling performance. The choice of
materials was primarily based on the (electro-)chemical and
mechanical matching of the components instead of solely
focusing on high-performance of individual components. Thus,
the battery utilized a phosphate backbone in combination
with tailored morphology of the electrode materials to
ensure good interfacial matching for a durable mechanical
stability. Moreover, the operating voltage range of the
active materials matches with the intrinsic electrochemical
window of the electrolyte which resulted in high
electrochemical stability. A highly competitive discharge
capacity of 63.5 mAh g–1 at 0.39 C after 500 cycles,
corresponding to $84\%$ of the initial discharge capacity,
was achieved. The analysis of interfacial charge transfer
kinetics confirmed the structural and electrical properties
of the electrodes and their interfaces with the electrolyte,
as evidenced by the excellent cycling performance of the
all-phosphate solid-state battery. These interfaces have
been studied via impedance analysis with subsequent
distribution of relaxation times analysis. Moreover, the
prepared solid-state battery could be processed and operated
in air atmosphere owing to the low oxygen sensitivity of the
phosphate materials. The analysis of electrolyte/electrode
interfaces after cycling demonstrates that the interfaces
remained stable during cycling.},
cin = {IEK-9},
ddc = {540},
cid = {I:(DE-Juel1)IEK-9-20110218},
pnm = {131 - Electrochemical Storage (POF3-131)},
pid = {G:(DE-HGF)POF3-131},
typ = {PUB:(DE-HGF)16},
pubmed = {pmid:29894641},
UT = {WOS:000438179000055},
doi = {10.1021/acsami.8b05902},
url = {https://juser.fz-juelich.de/record/851351},
}