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@ARTICLE{Napso:851478,
author = {Napso, Sofia and Rein, Dmitry M. and Fu, Zhendong and
Radulescu, Aurel and Cohen, Yachin},
title = {{S}tructural {A}nalysis of {C}ellulose-{C}oated
{O}il-in-{W}ater {E}mulsions {F}abricated from {M}olecular
{S}olution},
journal = {Langmuir},
volume = {34},
number = {30},
issn = {1520-5827},
address = {Washington, DC},
publisher = {ACS Publ.},
reportid = {FZJ-2018-05114},
pages = {8857 - 8865},
year = {2018},
abstract = {Natural cellulose has been used as a coating to stabilize
oil-in-water (o/w) emulsions by exploiting the amphiphilic
character of the cellulose chains molecularly dissolved in
the ionic liquid 1-ethyl-3-methylimidazolium acetate. Its
cellulose coating exhibits a continuous amorphous structure
which differs significantly from the cellulose particle
stabilization used in Pickering emulsions. The structure of
these cellulose-coated o/w emulsion particles, in particular
the cellulose coating shell characteristics (thickness,
porosity, and composition), is studied by using a
combination of direct imaging methods such as cryogenic
electron microscopy and fluorescence microscopy with
small-angle neutron scattering measurements. This work
suggests a unique multicompartment structure of the emulsion
particles: an oil core, surrounded by an inner shell
composed of a porous cellulose gel, encapsulated by a dense
outer cellulose shell, a few nanometers in thickness. The
thickness of the inner cellulose shell varies significantly.
The nanoscale emulsion droplets exhibit a thickness of 10 ±
3 nm, whereas the larger micron-sized droplets exhibit a
thicker inner cellulose shell of 500–750 nm. It is also
inferred that the cellulose shells contain water rather than
oil.},
cin = {JCNS (München) ; Jülich Centre for Neutron Science JCNS
(München) ; JCNS-FRM-II / Neutronenstreuung ; JCNS-1},
ddc = {670},
cid = {I:(DE-Juel1)JCNS-FRM-II-20110218 /
I:(DE-Juel1)JCNS-1-20110106},
pnm = {6G15 - FRM II / MLZ (POF3-6G15) / 6G4 - Jülich Centre for
Neutron Research (JCNS) (POF3-623)},
pid = {G:(DE-HGF)POF3-6G15 / G:(DE-HGF)POF3-6G4},
experiment = {EXP:(DE-MLZ)KWS2-20140101 / EXP:(DE-MLZ)KWS3-20140101},
typ = {PUB:(DE-HGF)16},
pubmed = {pmid:29979601},
UT = {WOS:000440768400016},
doi = {10.1021/acs.langmuir.8b01325},
url = {https://juser.fz-juelich.de/record/851478},
}