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@ARTICLE{Gelissen:851479,
author = {Gelissen, Arjan P. H. and Scotti, Andrea and Turnhoff,
Sarah K. and Janssen, Corinna and Radulescu, Aurel and Pich,
Andrij and Rudov, Andrey A. and Potemkin, Igor I. and
Richtering, Walter},
title = {{A}n anionic shell shields a cationic core allowing for
uptake and release of polyelectrolytes within core–shell
responsive microgels},
journal = {Soft matter},
volume = {14},
number = {21},
issn = {1744-6848},
address = {London},
publisher = {Royal Soc. of Chemistry},
reportid = {FZJ-2018-05115},
pages = {4287 - 4299},
year = {2018},
abstract = {To realize carriers for drug delivery, cationic containers
are required for anionic guests. Nevertheless, the toxicity
of cationic carriers limits their practical use. In this
study, we investigate a model system of polyampholyte
N-isopropylacrylamide (NIPAM)-based microgels with a
cationic core and an anionic shell to study whether the
presence of a negative shell allows the cationic core to be
shielded while still enabling the uptake and release of the
anionic guest polyelectrolytes. These microgels are loaded
with polystyrene sulfonate of different molecular weights to
investigate the influence of their chain length on the
uptake and release process. By means of small-angle neutron
scattering, we evaluate the spatial distribution of
polystyrene sulfonate within the microgels. The guest
molecules are located in different parts of the core–shell
microgels depending on their size. By combining these
scattering results with UV-vis spectroscopy, electrophoretic
mobility and potentiometric titrations we gain complementary
results to investigate the uptake and release process of
polyelectrolytes in polyampholyte core–shell microgels.
Moreover, Brownian molecular dynamic simulations are
performed to compare the experimental and theoretical
results of this model. Our findings demonstrate that the
presence of a shell still enables efficient uptake of guest
molecules into the cationic core. These anionic guest
molecules can be released through an anionic shell.
Furthermore, the presence of a shell enhances the stability
of the microgel–polyelectrolyte complexes with respect to
the cationic precursor microgel alone.},
cin = {JCNS (München) ; Jülich Centre for Neutron Science JCNS
(München) ; JCNS-FRM-II / Neutronenstreuung ; JCNS-1},
ddc = {530},
cid = {I:(DE-Juel1)JCNS-FRM-II-20110218 /
I:(DE-Juel1)JCNS-1-20110106},
pnm = {6G15 - FRM II / MLZ (POF3-6G15) / 6G4 - Jülich Centre for
Neutron Research (JCNS) (POF3-623)},
pid = {G:(DE-HGF)POF3-6G15 / G:(DE-HGF)POF3-6G4},
experiment = {EXP:(DE-MLZ)KWS2-20140101},
typ = {PUB:(DE-HGF)16},
pubmed = {pmid:29774926},
UT = {WOS:000434244800007},
doi = {10.1039/C8SM00397A},
url = {https://juser.fz-juelich.de/record/851479},
}