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@ARTICLE{Doppler:851498,
author = {Doppler, M. C. and Fleig, J. and Bram, M. and Opitz, A. K.},
title = {{H}ydrogen oxidation mechanisms on {N}i/yttria stabilized
zirconia anodes: {S}eparation of reaction pathways by
geometry variation of pattern electrodes},
journal = {Journal of power sources},
volume = {380},
issn = {0378-7753},
address = {New York, NY [u.a.]},
publisher = {Elsevier},
reportid = {FZJ-2018-05124},
pages = {46 - 54},
year = {2018},
abstract = {Nickel/yttria stabilized zirconia (YSZ) electrodes are
affecting the overall performance of solid oxide fuel cells
(SOFCs) in general and strongly contribute to the cell
resistance in case of novel metal supported SOFCs in
particular. The electrochemical fuel conversion mechanisms
in these electrodes are, however, still only partly
understood. In this study, micro-structured Ni thin film
electrodes on YSZ with 15 different geometries are utilized
to investigate reaction pathways for the hydrogen
electro-oxidation at Ni/YSZ anodes. From electrodes with
constant area but varying triple phase boundary (TPB) length
a contribution to the electro-catalytic activity is found
that does not depend on the TPB length. This additional
activity could clearly be attributed to a yet unknown
reaction pathway scaling with the electrode area. It is
shown that this area related pathway has significantly
different electrochemical behavior compared to the TPB
pathway regarding its thermal activation, sulfur poisoning
behavior, and H2/H2O partial pressure dependence. Moreover,
possible reaction mechanisms of this reaction pathway are
discussed, identifying either a pathway based on hydrogen
diffusion through Ni with water release at the TPB or a path
with oxygen diffusion through Ni to be a very likely
explanation for the experimental results.},
cin = {IEK-1},
ddc = {620},
cid = {I:(DE-Juel1)IEK-1-20101013},
pnm = {135 - Fuel Cells (POF3-135) / SOFC - Solid Oxide Fuel Cell
(SOFC-20140602)},
pid = {G:(DE-HGF)POF3-135 / G:(DE-Juel1)SOFC-20140602},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000440265800011},
doi = {10.1016/j.jpowsour.2018.01.073},
url = {https://juser.fz-juelich.de/record/851498},
}