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@PHDTHESIS{Caron:851773,
author = {Caron, Jan},
title = {{M}odel-based reconstruction of magnetisation distributions
in nanostructures from electron optical phase images},
volume = {177},
school = {RWTH Aachen},
type = {Dr},
address = {Jülich},
publisher = {Forschungszentrum Jülich GmbH Zentralbibliothek, Verlag},
reportid = {FZJ-2018-05288},
isbn = {978-3-95806-346-4},
series = {Schriften des Forschungszentrums Jülich. Reihe
Schlüsseltechnologien / Key Technologies},
pages = {XXI, 183 S.},
year = {2018},
note = {RWTH Aachen, Diss., 2017},
abstract = {Off-axis electron holography is a powerful technique for
recording the phase shift of high-energy electron waves that
pass through a thin specimen in the transmission electron
microscope. Information about the electromagnetic field in
and around the specimen is encoded in the phase, according
to the Aharonov-Bohm equations. In this thesis, a
model-based iterative reconstruction (MBIR) algorithm was
developed, which allows the retrieval of the projected
in-plane magnetisation distribution from individual magnetic
phase images or a complete tomographic reconstruction of the
three-dimensional magnetisation distribution from two
ideally orthogonal tilt series of phase images. To guarantee
efficient model-based reconstructions, an optimised forward
model implementation for fast and accurate simulations of
magnetic phase images from a given magnetisation
distribution was derived. This new approach utilises sparse
matrix multiplications and fast convolutions in Fourier
space with pre-calculated convolution kernels based on known
analytic solutions for the phase contribution of simple
geometries. As the inverse problem of retrieving the
magnetisation distribution is ill-posed, regularisation
techniques had to be applied, that guarantee the existence
of a solution and its uniqueness. Modelled after the
minimisation of the exchange energy, Tikhonov regularisation
of first order is used to apply smoothness constraints to
the solution of the reconstruction. In addition, $\textit{a
priori}$ knowledge about the position and size of the
magnetised regions is utilised in the form of a
three-dimensional mask to significantly reduce the number of
retrieval targets. Optimal estimation diagnostic tools were
adapted for the assessment of the quality of the
reconstruction results. The MBIR algorithm was successfully
applied to simulated phase images for the reconstruction of
two-and three-dimensional magnetisation distributions.
External sources of magnetisation outside the field of view
were addressed by linear phase ramp and offset fits, as well
as with buffer pixels that increase the number of degrees of
freedom for the MBIR algorithm. A method to account for the
perturbed reference wave of the electron hologram was
provided and other artefacts in the magnetic phase images
were tackled by excluding them from the reconstruction
process. In three dimensions, studies about the influence of
the maximum tilt angle and angular sampling were performed.
The MBIR algorithm was successfully used to reconstruct a
projected in-plane magnetisation distribution from a
magnetic phase image of a lithographically patterned cobalt
structure. Finally, a three-dimensional magnetisation
distribution was reconstructed from a set of simulated phase
images with limited angular range under the influence of
Gaussian noise and random phase offsets and ramps, proving
the feasibility of the algorithm for future
three-dimensional experimental studies.},
cin = {ER-C-2},
cid = {I:(DE-Juel1)ER-C-2-20170209},
pnm = {899 - ohne Topic (POF3-899)},
pid = {G:(DE-HGF)POF3-899},
typ = {PUB:(DE-HGF)3 / PUB:(DE-HGF)11},
url = {https://juser.fz-juelich.de/record/851773},
}