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@ARTICLE{Viani:852480,
      author       = {Viani, Alberto and Ševčík, Radek and Appavou,
                      Marie-Sousai and Radulescu, Aurel},
      title        = {{E}volution of fine microstructure during firing of
                      extruded clays: {A} small angle neutron scattering study},
      journal      = {Applied clay science},
      volume       = {166},
      issn         = {0169-1317},
      address      = {New York, NY [u.a.]},
      publisher    = {Elsevier},
      reportid     = {FZJ-2018-05411},
      pages        = {1 - 8},
      year         = {2018},
      abstract     = {The microstructure of extruded fired-clay bodies in the
                      interval 800–1100 °C has been investigated with small
                      angle neutron scattering. The evolution of the retrieved
                      pore size distribution is compatible with the coarsening of
                      the pore network with increasing temperature. The analysis
                      of the scattering curves in combination with results of
                      electron microscopy, indicated a multiscale nature for the
                      pore-matrix microstructure. A structural parameter obtained
                      from the analysis of the scattering curves, is proposed as
                      indicator of maximum firing temperature through the
                      implementation of a linear calibration curve. Such method
                      has been successfully tested on a material of industrial
                      production and can be considered of interest for the
                      production of custom made replacement materials in the
                      conservation of cultural heritage or for the
                      characterization of the manufacturing process of
                      archaeological fired-clay objects. Textural features
                      originated by the forming process of extrusion have been
                      detected as anisotropy of the pore network. They are still
                      present above 1000 °C and, because of the use of screw
                      extrusion, they are observed in both sections cut parallel
                      and perpendicular to the direction of extrusion.},
      cin          = {JCNS (München) ; Jülich Centre for Neutron Science JCNS
                      (München) ; JCNS-FRM-II / Neutronenstreuung ; JCNS-1},
      ddc          = {550},
      cid          = {I:(DE-Juel1)JCNS-FRM-II-20110218 /
                      I:(DE-Juel1)JCNS-1-20110106},
      pnm          = {6G15 - FRM II / MLZ (POF3-6G15) / 6G4 - Jülich Centre for
                      Neutron Research (JCNS) (POF3-623)},
      pid          = {G:(DE-HGF)POF3-6G15 / G:(DE-HGF)POF3-6G4},
      experiment   = {EXP:(DE-MLZ)KWS2-20140101},
      typ          = {PUB:(DE-HGF)16},
      UT           = {WOS:000449135300001},
      doi          = {10.1016/j.clay.2018.09.002},
      url          = {https://juser.fz-juelich.de/record/852480},
}