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@PHDTHESIS{Green:852905,
author = {Green, Matthew Felix Blishen},
title = {{C}reating and characterizing a single molecule device for
quantitative surface science},
volume = {181},
school = {RWTH Aachen},
type = {Dr.},
address = {Jülich},
publisher = {Forschungszentrum Jülich GmbH Zentralbibliothek, Verlag},
reportid = {FZJ-2018-05692},
isbn = {978-3-95806-352-5},
series = {Schriften des Forschungszentrums Jülich. Reihe
Schlüsseltechnologien / Key Technologies},
pages = {getr. Zählung},
year = {2018},
note = {RWTH Aachen, Diss., 2018},
abstract = {This thesis has presented the creation and characterization
of a single molecule device. A new microscopy method, SQDM,
was developed and shown to be capable of measuring local
electrostatic potential in a truly quantitative fashion. The
nature of the single molecule sensor itself was investigated
in-depth and unexpected results were achieved, contradicting
the predictions of the highly successful orthodox theory of
the Coulomb blockade. The single molecule device was
constructed with the use of atomically precise single
molecule manipulation detailed in Chap. 2. Approaching the
microscope tip towards a single molecule, a covalent bond
was formed between the apex atom of the tip and one of the
double-bonded corner oxygen atoms of the molecule. This bond
was empirically found to be strong enough to remove the
molecule not only from its chemisorbed state on the surface,
but from its hydrogen-bonded molecular layer. The removals
were made possible by the augmentation of the SPM setup with
a three-dimensional motion tracking device, which was used
to explore custom removal trajectories by selective
variation. Since the molecule’s geometry was controlled
throughout the manipulation process, it was thereafter
possible to re-deposit the molecule to the surface by
re-approaching and applying a voltage pulse. Using this
protocol, the word ‘JÜLICH’ was patterned into a PTCDA
monolayer by removing molecules one by one. The correction
of a mistake in the patterning was also demonstrated by
lowering a molecule into a previously created vacancy.
Currently work is underway to further the understanding of
the key parameters involved in successful removal
trajectories. Next, the functionality of the single molecule
device was exhibited in Chap. 3 with the development of
SQDM. It was shown that the molecular QD was sufficiently
electronically decoupled from the tip’s electronic states
that integer charge could be stabilized on it: the presence
of resonant tunnelling features as well as sudden changes in
the tip-sample force were the signals of single electron
charging. The [...]},
cin = {PGI-3},
cid = {I:(DE-Juel1)PGI-3-20110106},
pnm = {142 - Controlling Spin-Based Phenomena (POF3-142)},
pid = {G:(DE-HGF)POF3-142},
typ = {PUB:(DE-HGF)3 / PUB:(DE-HGF)11},
url = {https://juser.fz-juelich.de/record/852905},
}