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000856723 1001_ $$0P:(DE-HGF)0$$aPérigo, Élio A$$b0$$eCorresponding author
000856723 245__ $$aEffect of annealing conditions on the microstructure and magnetic properties of sintered Nd-Fe-B magnets as seen by magnetic small-angle neutron scatteringml
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000856723 520__ $$aWe have investigated the effect of the annealing conditions (heating rate and temperature) on themagnetic microstructure of sintered Nd-Fe-B magnets by means of magnetometry, scanning electronmicroscopy, high-energy synchrotron x-ray diffraction, and small-angle neutron scattering (SANS).While the temperature treatment has a strong effect on the coercivity (reduction by about 50% onannealing), the associated changes in the microstructure do surprisingly not show up (or at best onlyvery weakly) in the neutron-scattering signal, which probes a mesoscopic real-space length scaleranging between about 1–300 nm. On the other hand, the x-ray data reveal microstructural changes inthe Nd-rich phases, presumably due to modifications in grain-boundary regions. Moreover, weobserve an unusual diamond-shaped angular anisotropy in the SANS cross section, which stronglypoints towards the existence of texture in the nuclear microstructure.
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000856723 7001_ $$0P:(DE-HGF)0$$aTitov, Ivan$$b1
000856723 7001_ $$0P:(DE-HGF)0$$aWeber, Raoul$$b2
000856723 7001_ $$0P:(DE-HGF)0$$aMettus, Denis$$b3
000856723 7001_ $$0P:(DE-HGF)0$$aPeral, Inma$$b4
000856723 7001_ $$0P:(DE-HGF)0$$aVallcorba, Oriol$$b5
000856723 7001_ $$0P:(DE-HGF)0$$aHonecker, Dirk$$b6
000856723 7001_ $$0P:(DE-Juel1)144382$$aFeoktystov, Artem$$b7$$ufzj
000856723 7001_ $$00000-0002-2786-295X$$aMichels, Andreas$$b8
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