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@ARTICLE{Prigo:856723,
author = {Périgo, Élio A and Titov, Ivan and Weber, Raoul and
Mettus, Denis and Peral, Inma and Vallcorba, Oriol and
Honecker, Dirk and Feoktystov, Artem and Michels, Andreas},
title = {{E}ffect of annealing conditions on the microstructure and
magnetic properties of sintered {N}d-{F}e-{B} magnets as
seen by magnetic small-angle neutron scatteringml},
journal = {Materials Research Express},
volume = {5},
number = {3},
issn = {2053-1591},
address = {Bristol},
publisher = {IOP Publ.},
reportid = {FZJ-2018-06074},
pages = {036110 -},
year = {2018},
abstract = {We have investigated the effect of the annealing conditions
(heating rate and temperature) on themagnetic microstructure
of sintered Nd-Fe-B magnets by means of magnetometry,
scanning electronmicroscopy, high-energy synchrotron x-ray
diffraction, and small-angle neutron scattering (SANS).While
the temperature treatment has a strong effect on the
coercivity (reduction by about $50\%$ onannealing), the
associated changes in the microstructure do surprisingly not
show up (or at best onlyvery weakly) in the
neutron-scattering signal, which probes a mesoscopic
real-space length scaleranging between about 1–300 nm. On
the other hand, the x-ray data reveal microstructural
changes inthe Nd-rich phases, presumably due to
modifications in grain-boundary regions. Moreover,
weobserve an unusual diamond-shaped angular anisotropy in
the SANS cross section, which stronglypoints towards the
existence of texture in the nuclear microstructure.},
cin = {JCNS-FRM-II / JCNS-2},
ddc = {620},
cid = {I:(DE-Juel1)JCNS-FRM-II-20110218 /
I:(DE-Juel1)JCNS-2-20110106},
pnm = {6G4 - Jülich Centre for Neutron Research (JCNS) (POF3-623)
/ 6G15 - FRM II / MLZ (POF3-6G15)},
pid = {G:(DE-HGF)POF3-6G4 / G:(DE-HGF)POF3-6G15},
experiment = {EXP:(DE-MLZ)KWS1-20140101},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000428807900001},
doi = {10.1088/2053-1591/aab7aa},
url = {https://juser.fz-juelich.de/record/856723},
}