000857256 001__ 857256 000857256 005__ 20240712100953.0 000857256 0247_ $$2doi$$a10.1002/rcm.8228 000857256 0247_ $$2ISSN$$a0951-4198 000857256 0247_ $$2ISSN$$a1097-0231 000857256 0247_ $$2altmetric$$aaltmetric:44483725 000857256 0247_ $$2pmid$$apmid:29971833 000857256 0247_ $$2WOS$$aWOS:000478091100008 000857256 037__ $$aFZJ-2018-06485 000857256 082__ $$a530 000857256 1001_ $$00000-0002-8500-8903$$aSchramm, Sébastien$$b0$$eCorresponding author 000857256 245__ $$aNew application of direct analysis in real time high-resolution mass spectrometry for the untargeted analysis of fresh and aged secondary organic aerosols generated from monoterpenes 000857256 260__ $$aNew York, NY$$bWiley Interscience$$c2019 000857256 3367_ $$2DRIVER$$aarticle 000857256 3367_ $$2DataCite$$aOutput Types/Journal article 000857256 3367_ $$0PUB:(DE-HGF)16$$2PUB:(DE-HGF)$$aJournal Article$$bjournal$$mjournal$$s1559040334_27224 000857256 3367_ $$2BibTeX$$aARTICLE 000857256 3367_ $$2ORCID$$aJOURNAL_ARTICLE 000857256 3367_ $$00$$2EndNote$$aJournal Article 000857256 520__ $$aRationaleSecondary organic aerosols (SOAs) represent a significant portion of total atmospheric aerosols. They are generated by the oxidation of volatile organic compounds (VOCs), and particularly biogenic VOCs (BVOCs). The analysis of such samples is usually performed by targeted methods that often require time‐consuming preparation steps that can induce loss of compounds and/or sample contaminations.MethodsRecently, untargeted methods using high‐resolution mass spectrometry (HRMS) have been successfully employed for a broad characterization of chemicals in SOAs. Herein we propose a new application of the direct analysis in real time (DART) ionization method combined with HRMS to quickly detect several hundred chemicals in SOAs collected on a quartz filter without sample preparation or separation techniques.ResultsThe reproducibility of measurements was good, with several hundred elemental compositions common to three different replicates. The relative standard deviations of the intensities of the chemical families ranged from 6% to 35%, with sufficient sensitivity to allow the unambiguous detection of 4 ng/mm2 of pinic acid. The presence of oligomers and specific tracers was highlighted by MSn (n ≤ 4) experiments, an achievement that is difficult to attain with other ultrahigh‐resolution mass spectrometers. Contributions of this untargeted DART‐HRMS method were illustrated by the analysis of fresh and aged SOAs from different gaseous precursors such as limonene, a β‐pinene/limonene mixture or scots pines emissions.ConclusionsThe results show that it is possible to use DART‐HRMS for the identification of tracers of specific aging reactions, or for the identification of aerosols from specific biogenic precursors. 000857256 536__ $$0G:(DE-HGF)POF3-243$$a243 - Tropospheric trace substances and their transformation processes (POF3-243)$$cPOF3-243$$fPOF III$$x0 000857256 588__ $$aDataset connected to CrossRef 000857256 7001_ $$0P:(DE-HGF)0$$aZannoni, Nora$$b1 000857256 7001_ $$0P:(DE-HGF)0$$aGros, Valérie$$b2 000857256 7001_ $$0P:(DE-Juel1)5344$$aTillmann, Ralf$$b3$$ufzj 000857256 7001_ $$0P:(DE-Juel1)4528$$aKiendler-Scharr, Astrid$$b4$$ufzj 000857256 7001_ $$0P:(DE-HGF)0$$aSarda-Estève, Roland$$b5 000857256 7001_ $$0P:(DE-HGF)0$$aBridoux, Maxime$$b6 000857256 773__ $$0PERI:(DE-600)2002158-6$$a10.1002/rcm.8228$$nS1$$p50-59$$tRapid communications in mass spectrometry$$v33$$x0951-4198$$y2019 000857256 8564_ $$uhttps://juser.fz-juelich.de/record/857256/files/Schramm_et_al-2019-Rapid_Communications_in_Mass_Spectrometry.pdf$$yRestricted 000857256 8564_ $$uhttps://juser.fz-juelich.de/record/857256/files/Schramm_et_al-2019-Rapid_Communications_in_Mass_Spectrometry.pdf?subformat=pdfa$$xpdfa$$yRestricted 000857256 909CO $$ooai:juser.fz-juelich.de:857256$$pVDB:Earth_Environment$$pVDB 000857256 9101_ $$0I:(DE-588b)5008462-8$$6P:(DE-Juel1)5344$$aForschungszentrum Jülich$$b3$$kFZJ 000857256 9101_ $$0I:(DE-588b)5008462-8$$6P:(DE-Juel1)4528$$aForschungszentrum Jülich$$b4$$kFZJ 000857256 9131_ $$0G:(DE-HGF)POF3-243$$1G:(DE-HGF)POF3-240$$2G:(DE-HGF)POF3-200$$3G:(DE-HGF)POF3$$4G:(DE-HGF)POF$$aDE-HGF$$bErde und Umwelt$$lAtmosphäre und Klima$$vTropospheric trace substances and their transformation processes$$x0 000857256 9141_ $$y2019 000857256 915__ $$0StatID:(DE-HGF)0420$$2StatID$$aNationallizenz 000857256 915__ $$0StatID:(DE-HGF)0200$$2StatID$$aDBCoverage$$bSCOPUS 000857256 915__ $$0StatID:(DE-HGF)0300$$2StatID$$aDBCoverage$$bMedline 000857256 915__ $$0StatID:(DE-HGF)0310$$2StatID$$aDBCoverage$$bNCBI Molecular Biology Database 000857256 915__ $$0StatID:(DE-HGF)0100$$2StatID$$aJCR$$bRAPID COMMUN MASS SP : 2017 000857256 915__ $$0StatID:(DE-HGF)0600$$2StatID$$aDBCoverage$$bEbsco Academic Search 000857256 915__ $$0StatID:(DE-HGF)0030$$2StatID$$aPeer Review$$bASC 000857256 915__ $$0StatID:(DE-HGF)0199$$2StatID$$aDBCoverage$$bClarivate Analytics Master Journal List 000857256 915__ $$0StatID:(DE-HGF)0110$$2StatID$$aWoS$$bScience Citation Index 000857256 915__ $$0StatID:(DE-HGF)0150$$2StatID$$aDBCoverage$$bWeb of Science Core Collection 000857256 915__ $$0StatID:(DE-HGF)0111$$2StatID$$aWoS$$bScience Citation Index Expanded 000857256 915__ $$0StatID:(DE-HGF)1150$$2StatID$$aDBCoverage$$bCurrent Contents - Physical, Chemical and Earth Sciences 000857256 915__ $$0StatID:(DE-HGF)1050$$2StatID$$aDBCoverage$$bBIOSIS Previews 000857256 915__ $$0StatID:(DE-HGF)9900$$2StatID$$aIF < 5 000857256 9201_ $$0I:(DE-Juel1)IEK-8-20101013$$kIEK-8$$lTroposphäre$$x0 000857256 980__ $$ajournal 000857256 980__ $$aVDB 000857256 980__ $$aI:(DE-Juel1)IEK-8-20101013 000857256 980__ $$aUNRESTRICTED 000857256 981__ $$aI:(DE-Juel1)ICE-3-20101013