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@ARTICLE{Wrana:857762,
author = {Wrana, Dominik and Rodenbücher, Christian and Jany,
Benedykt R. and Kryshtal, Oleksandr and Cempura, Grzegorz
and Kruk, Adam and Indyka, Paulina and Szot, Krzysztof and
Krok, Franciszek},
title = {{A} bottom-up process of self-formation of highly
conductive titanium oxide ({T}i{O}) nanowires on reduced
{S}r{T}i{O} 3},
journal = {Nanoscale},
volume = {11},
number = {1},
issn = {2040-3372},
address = {Cambridge},
publisher = {RSC Publ.},
reportid = {FZJ-2018-06730},
pages = {89-97},
year = {2019},
abstract = {Reduced titanium oxide structures are regarded as promising
materials for various catalytic and optoelectronic
applications. There is thus an urgent need for developing
methods of controllable formation of crystalline
nanostructures with tunable oxygen nonstoichiometry. We
introduce the Extremely Low Oxygen Partial Pressure (ELOP)
method, employing an oxygen getter in close vicinity to an
oxide during thermal reduction under vacuum, as an effective
bottom-up method for the production of nanowires arranged in
a nanoscale metallic network on a SrTiO3 perovskite surface.
We demonstrate that the TiO nanowires crystallize in a
highly ordered cubic phase, where single nanowires are
aligned along the main crystallographic directions of the
SrTiO3 substrate. The dimensions of the nanostructures are
easily tunable from single nanometers up to the mesoscopic
range by varying the temperature of reduction. The interface
between TiO and SrTiO3 (metal and insulator) was found to be
atomically sharp providing the unique possibility of the
investigation of electronic states, especially since the
high conductivity of the TiO nanostructures is maintained
after room temperature oxidation. According to the growth
model we propose, TiO nanowire formation is possible due to
the incongruent sublimation of strontium and
crystallographic shearing, triggered by the extremely low
oxygen partial pressure (ELOP). The controlled formation of
conductive nanowires on a perovskite surface holds
technological potential for implementation in memristive
devices, organic electronics, or for catalytic applications,
and provides insight into the mechanism of nanoscale phase
transformations in metal oxides. We believe that the ELOP
mechanism of suboxide formation is suitable for the
formation of reduced suboxides on other perovskite oxides
and for the broader class of transition metal oxides.},
cin = {PGI-7 / JARA-FIT},
ddc = {600},
cid = {I:(DE-Juel1)PGI-7-20110106 / $I:(DE-82)080009_20140620$},
pnm = {521 - Controlling Electron Charge-Based Phenomena
(POF3-521)},
pid = {G:(DE-HGF)POF3-521},
typ = {PUB:(DE-HGF)16},
pubmed = {pmid:30226243},
UT = {WOS:000454327500036},
doi = {10.1039/C8NR04545C},
url = {https://juser.fz-juelich.de/record/857762},
}