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@ARTICLE{Grnebaum:857797,
author = {Grünebaum, Mariano and Buchheit, Annika and Krause, Daniel
and Hiller, Martin Manuel and Schmidt, Christina and Winter,
Martin and Wiemhöfer, Hans-Dieter},
title = {{D}evelopment of new pyrazole-based lithium salts for
battery applications – {D}o established basic design
concepts really work?},
journal = {Electrochimica acta},
volume = {286},
issn = {0013-4686},
address = {New York, NY [u.a.]},
publisher = {Elsevier},
reportid = {FZJ-2018-06764},
pages = {313 - 323},
year = {2018},
abstract = {This work is focused on applying structural concepts and
basic chemical principles to model two N-heterocyclic
lithium salts, based on trifluoromethyl substituted
pyrazolide anions. An easily upscalable preparation method
without difficult purification steps was also developed. In
a comparative study, the physicochemical properties of the
two new lithium salts were investigated, particularly the
effect of an additional BF3-group at the nitrogen atom. In
comparison to non-substituted lithium pyrazolide, the
BF3-addition led to a strong improvement of thermal and
electrochemical stability, ionic conductivity, as well as
better C-rate and cycling performance. Furthermore, the
anodic stability of Al current collectors was investigated
and compared to commercial lithium salts, namely LiPF6 and
lithium bis((trifluoromethyl)sulfonyl)imide (LiTFSI).
Possible mechanisms that lead to the presented improvements
are discussed.},
cin = {IEK-12},
ddc = {540},
cid = {I:(DE-Juel1)IEK-12-20141217},
pnm = {131 - Electrochemical Storage (POF3-131)},
pid = {G:(DE-HGF)POF3-131},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000445133700036},
doi = {10.1016/j.electacta.2018.08.055},
url = {https://juser.fz-juelich.de/record/857797},
}