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000858473 041__ $$aEnglish
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000858473 1001_ $$0P:(DE-HGF)0$$aHodgkinson, Paul$$b0$$eEditor
000858473 245__ $$aChapter 10. Isotopically Enriched Systems
000858473 260__ $$aLondon$$bRoyal Society of Chemistry$$c2018
000858473 29510 $$aModern methods in solid-state NMR : a practitioner's guide / Hodgkinson, Paul , London : Royal Society of Chemistry, 2018,
000858473 300__ $$axvi, 435 Seiten : illustrations
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000858473 3367_ $$0PUB:(DE-HGF)7$$2PUB:(DE-HGF)$$aContribution to a book$$bcontb$$mcontb$$s1544722738_2055
000858473 4900_ $$aNew developments in NMR$$vNo. 15
000858473 520__ $$aMost solid-state NMR measurements employ rare-spin nuclei, such as 13C or 15N, for detection. However, the low natural abundance of those spins limits the possibility of obtaining multidimensional homo- or hetero-nuclear solid-state NMR-spectra, which rely on internuclear correlations between those rare spins, unless signal enhancement or isotopic labelling is applied. In this chapter, we first give an overview of different techniques for selective and uniform isotope labelling of biomolecules. In the following sections, we describe different homo- and hetero-nuclear recoupling techniques and their use in multidimensional NMR spectroscopy. In particular, we emphasize the difference between zeroth-order recoupling techniques, which are well-suited for dipolar transfers between spins close in space, and second- and higher-order recoupling schemes, which allow the detection of long-range correlations. We also provide some examples how these techniques are applied towards structure elucidation of biomolecules. Finally, we briefly outline the technique of signal enhancement by dynamic nuclear polarization, a method that may in part help to overcome the need for isotopic enrichment.
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000858473 7001_ $$0P:(DE-Juel1)137006$$aBeumer, Claudia$$b1
000858473 7001_ $$0P:(DE-Juel1)165604$$aSchölzel, Daniel$$b2$$ufzj
000858473 7001_ $$0P:(DE-Juel1)165994$$aKönig, Anna$$b3$$ufzj
000858473 7001_ $$0P:(DE-Juel1)161489$$aUluca, Boran$$b4$$ufzj
000858473 7001_ $$0P:(DE-Juel1)161487$$aWeirich, Franziska$$b5
000858473 7001_ $$0P:(DE-Juel1)132002$$aHeise, Henrike$$b6$$eCorresponding author$$ufzj
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