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@INBOOK{Hodgkinson:858473,
      author       = {Beumer, Claudia and Schölzel, Daniel and König, Anna and
                      Uluca, Boran and Weirich, Franziska and Heise, Henrike},
      editor       = {Hodgkinson, Paul},
      title        = {{C}hapter 10. {I}sotopically {E}nriched {S}ystems},
      volume       = {No. 15},
      address      = {London},
      publisher    = {Royal Society of Chemistry},
      reportid     = {FZJ-2018-07345},
      isbn         = {978-1-78801-046-7},
      series       = {New developments in NMR},
      pages        = {xvi, 435 Seiten : illustrations},
      year         = {2018},
      comment      = {Modern methods in solid-state NMR : a practitioner's guide
                      / Hodgkinson, Paul , London : Royal Society of Chemistry,
                      2018,},
      booktitle     = {Modern methods in solid-state NMR : a
                       practitioner's guide / Hodgkinson, Paul
                       , London : Royal Society of Chemistry,
                       2018,},
      abstract     = {Most solid-state NMR measurements employ rare-spin nuclei,
                      such as 13C or 15N, for detection. However, the low natural
                      abundance of those spins limits the possibility of obtaining
                      multidimensional homo- or hetero-nuclear solid-state
                      NMR-spectra, which rely on internuclear correlations between
                      those rare spins, unless signal enhancement or isotopic
                      labelling is applied. In this chapter, we first give an
                      overview of different techniques for selective and uniform
                      isotope labelling of biomolecules. In the following
                      sections, we describe different homo- and hetero-nuclear
                      recoupling techniques and their use in multidimensional NMR
                      spectroscopy. In particular, we emphasize the difference
                      between zeroth-order recoupling techniques, which are
                      well-suited for dipolar transfers between spins close in
                      space, and second- and higher-order recoupling schemes,
                      which allow the detection of long-range correlations. We
                      also provide some examples how these techniques are applied
                      towards structure elucidation of biomolecules. Finally, we
                      briefly outline the technique of signal enhancement by
                      dynamic nuclear polarization, a method that may in part help
                      to overcome the need for isotopic enrichment.},
      keywords     = {Festkörper-NMR-Spektroskopie (gnd)},
      cin          = {ICS-6},
      ddc          = {541.0421},
      cid          = {I:(DE-Juel1)ICS-6-20110106},
      pnm          = {551 - Functional Macromolecules and Complexes (POF3-551)},
      pid          = {G:(DE-HGF)POF3-551},
      typ          = {PUB:(DE-HGF)7},
      url          = {https://juser.fz-juelich.de/record/858473},
}