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@ARTICLE{Stuckart:858629,
author = {Stuckart, Maria and Izarova, Natalya V. and vanLeusen, Jan
and Smekhova, Alevtina and Schmitz-Antoniak, Carolin and
Bamberger, Heiko and vanSlageren, Joris and
Santiago-Schübel, Beatrix and Kögerler, Paul},
title = {{H}ost-{G}uest-{I}nduced {E}nvironment {T}uning of 3d
{I}ons in a {P}olyoxopalladate {M}atrix},
journal = {Chemistry - a European journal},
volume = {24},
number = {67},
issn = {0947-6539},
address = {Weinheim},
publisher = {Wiley-VCH},
reportid = {FZJ-2018-07489},
pages = {17767 - 17778},
year = {2018},
abstract = {A series of unprecedented supramolecular associates of
phenylarsonate‐capped {MIIPdII12O8}‐type (M=Co, Ni and
Zn) polyoxopalladates with α‐cyclodextrins (α‐CD) was
obtained and characterized in the solid state
(single‐crystal X‐ray diffraction (XRD), FT‐IR
spectroscopy, elemental and thermogravimetric (TGA)
analyses), in aqueous solution (1H and 13C NMR) and in the
gas phase (ESI‐MS). The non‐covalent host–guest
interactions between the organopolyoxoanions and α‐CD
rings alter the O8 coordination environment of a 3d
transition metal ion (MII) situated at the center of a
cuboid polyoxododecapalladate shell. This synthetically
controlled “chemical pressure” effectively induces axial
distortion of the otherwise cubic polyoxopalladate
environment between two trans‐positioned α‐CD moieties.
Its effect on the magnetic properties and the electronic
structure of the CoII derivative was assessed in a combined
SQUID magnetometry, EPR, X‐ray magnetic circular/linear
dichroism (XMCD/XMLD), and X‐ray absorption near‐edge
structure (XANES) spectroscopy study.},
cin = {PGI-6},
ddc = {540},
cid = {I:(DE-Juel1)PGI-6-20110106},
pnm = {522 - Controlling Spin-Based Phenomena (POF3-522)},
pid = {G:(DE-HGF)POF3-522},
typ = {PUB:(DE-HGF)16},
pubmed = {pmid:30261127},
UT = {WOS:000451888300021},
doi = {10.1002/chem.201803531},
url = {https://juser.fz-juelich.de/record/858629},
}