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@ARTICLE{Cao:859195,
author = {Cao, Lei and Petracic, Oleg and Zakalek, Paul and Weber,
Alexander and Rücker, Ulrich and Schubert, Jürgen and
Koutsioumpas, Alexandros and Mattauch, Stefan and Brückel,
Thomas},
title = {{R}eversible {C}ontrol of {P}hysical {P}roperties via an
{O}xygen-{V}acancy-{D}riven {T}opotactic {T}ransition in
{E}pitaxial {L}a 0.7 {S}r 0.3 {M}n{O} 3− δ {T}hin
{F}ilms},
journal = {Advanced materials},
volume = {31},
number = {7},
issn = {0935-9648},
address = {Weinheim},
publisher = {Wiley-VCH},
reportid = {FZJ-2019-00085},
pages = {1806183 -},
year = {2019},
abstract = {The vacancy distribution of oxygen and its dynamics
directly affect the functional response of complex oxides
and their potential applications. Dynamic control of the
oxygen composition may provide the possibility to
deterministically tune the physical properties and establish
a comprehensive understanding of the structure–property
relationship in such systems. Here, an
oxygen‐vacancy‐induced topotactic transition from
perovskite to brownmillerite and vice versa in epitaxial
La0.7Sr0.3MnO3−δ thin films is identified by real‐time
X‐ray diffraction. A novel intermediate phase with a
noncentered crystal structure is observed for the first time
during the topotactic phase conversion which indicates a
distinctive transition route. Polarized neutron
reflectometry confirms an oxygen‐deficient interfacial
layer with drastically reduced nuclear scattering length
density, further enabling a quantitative determination of
the oxygen stoichiometry (La0.7Sr0.3MnO2.65) for the
intermediate state. Associated physical properties of
distinct topotactic phases (i.e., ferromagnetic metal and
antiferromagnetic insulator) can be reversibly switched by
an oxygen desorption/absorption cycling process.
Importantly, a significant lowering of necessary conditions
(temperatures below 100 °C and conversion time less than 30
min) for the oxygen reloading process is found. These
results demonstrate the potential applications of defect
engineering in the design of perovskite‐based functional
materials.},
cin = {JCNS-2 / PGI-4 / JARA-FIT / JCNS-FRM-II / JCNS-HBS / PGI-9},
ddc = {660},
cid = {I:(DE-Juel1)JCNS-2-20110106 / I:(DE-Juel1)PGI-4-20110106 /
$I:(DE-82)080009_20140620$ /
I:(DE-Juel1)JCNS-FRM-II-20110218 /
I:(DE-Juel1)JCNS-HBS-20180709 / I:(DE-Juel1)PGI-9-20110106},
pnm = {144 - Controlling Collective States (POF3-144) / 524 -
Controlling Collective States (POF3-524) / 6212 - Quantum
Condensed Matter: Magnetism, Superconductivity (POF3-621) /
6213 - Materials and Processes for Energy and Transport
Technologies (POF3-621) / 6G4 - Jülich Centre for Neutron
Research (JCNS) (POF3-623)},
pid = {G:(DE-HGF)POF3-144 / G:(DE-HGF)POF3-524 /
G:(DE-HGF)POF3-6212 / G:(DE-HGF)POF3-6213 /
G:(DE-HGF)POF3-6G4},
experiment = {EXP:(DE-MLZ)MARIA-20140101},
typ = {PUB:(DE-HGF)16},
pubmed = {pmid:30570780},
UT = {WOS:000459724200012},
doi = {10.1002/adma.201806183},
url = {https://juser.fz-juelich.de/record/859195},
}